1,2-Dichloro-4-(phenylsulfanyl)benzene

Base Information

Chemical Name:1,2-Dichloro-4-(phenylsulfanyl)benzene
CAS No.:65662-89-7
Molecular Formula:C12H8Cl2S
Molecular Weight:255.168
Hs Code.:
DSSTox Substance ID:DTXSID40495799
Wikidata:Q82344157

Synonyms:65662-89-7;1,2-Dichloro-4-(phenylsulfanyl)benzene;DTXSID40495799

Suppliers and Price of 1,2-Dichloro-4-(phenylsulfanyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,2-Dichloro-4-(phenylsulfanyl)benzene

Chemical Property:

XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:253.9723768
Heavy Atom Count:15
Complexity:192

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)SC2=CC(=C(C=C2)Cl)Cl

Technology Process of 1,2-Dichloro-4-(phenylsulfanyl)benzene

There total 5 articles about 1,2-Dichloro-4-(phenylsulfanyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 4235-78-3
1,2-dichloro-4-[(3,4-dichlorophenyl)disulfanyl]benzene

: phenylzinc pivalate

: 65662-89-7
(3,4-dichlorophenyl)(phenyl)sulfane

Guidance literature:: With cobalt(II) chloride; In tetrahydrofuran; at 20 ℃; for 12h; Schlenk technique;
DOI:10.1021/acs.orglett.8b03319

Reference yield:

: 591-50-4
iodobenzene

: 5858-17-3
3,4-dichlorothiophenol

: 65662-89-7
(3,4-dichlorophenyl)(phenyl)sulfane

Guidance literature:: With potassium tert-butylate; C₂₂H₂₅BrN₃NiO₂; In N,N-dimethyl-formamide; at 100 ℃; for 19h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jcat.2020.01.016

Reference yield:

: 591-50-4
iodobenzene

: 65662-89-7
(3,4-dichlorophenyl)(phenyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1.1: TurboGrignard / tetrahydrofuran / -20 °C / Schlenk technique

1.2: 0.17 h / 0 - 25 °C / Schlenk technique

2.1: cobalt(II) chloride / tetrahydrofuran / 12 h / 20 °C / Schlenk technique

With TurboGrignard; cobalt(II) chloride; In tetrahydrofuran;
DOI:10.1021/acs.orglett.8b03319