2-Phenyl-1,2-benzoxazol-3-one

Base Information

Chemical Name:2-Phenyl-1,2-benzoxazol-3-one
CAS No.:65685-42-9
Molecular Formula:C13H9NO2
Molecular Weight:211.22
Hs Code.:
ChEMBL ID:CHEMBL1721811
DSSTox Substance ID:DTXSID90495709
Nikkaji Number:J1.288.479F
Wikidata:Q27164178

Synonyms:2-phenyl-1,2-benzoxazol-3-one;65685-42-9;2-Phenylbenzo[d]isoxazol-3(2H)-one;1,2-Benzisoxazol-3(2H)-one, 2-phenyl-;KUC103670N;MLS003116054;2-phenylindoxazen-3-one;CHEMBL1721811;BDBM61909;CHEBI:92443;DTXSID90495709;cid_12385463;KUC103670;2-Phenyl-1,2-benzoxazol-3(2H)-one;SMR001831609;F95300;Q27164178;Z2049888557

Suppliers and Price of 2-Phenyl-1,2-benzoxazol-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Phenyl-1,2-benzoxazol-3-one

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:211.063328530
Heavy Atom Count:16
Complexity:273

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C(=O)C3=CC=CC=C3O2

Technology Process of 2-Phenyl-1,2-benzoxazol-3-one

There total 2 articles about 2-Phenyl-1,2-benzoxazol-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 19393-60-3
N-phenyl-salicylohydroxamic acid

: 65685-42-9
2-phenylbenzol[d]isooxazol-3(2H)-one

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 25 ℃; for 0.5h;
DOI:10.1016/S0040-4039(00)00164-7

Reference yield:

: 50-78-2,98201-60-6
aspirin

: 65685-42-9
2-phenylbenzol[d]isooxazol-3(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: (COCl)2 / CH₂Cl₂ / 1 h / 25 °C / Heating

2: Na₂CO₃ / CH₂Cl₂; tetrahydrofuran / 1 h / 25 °C

3: 90 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 - 25 °C

With oxalyl dichloride; sodium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Acid chloride formation / 2: Substitution / 3: Dehydration;
DOI:10.1016/S0040-4039(00)00164-7