diethyl fluoro[4-(2-methylpropyl)phenyl]propanedioate

Base Information

Chemical Name:diethyl fluoro[4-(2-methylpropyl)phenyl]propanedioate
CAS No.:23197-71-9
Molecular Formula:C17H23 F O4
Molecular Weight:310.3605
Hs Code.:
Mol file:23197-71-9.mol

Synonyms:Malonicacid, fluoro(p-isobutylphenyl)-, diethyl ester (8CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl fluoro[4-(2-methylpropyl)phenyl]propanedioate

Chemical Property:

Vapor Pressure:9E-06mmHg at 25°C
Boiling Point:373.4°C at 760 mmHg
Flash Point:173.5°C
PSA：52.60000
Density:1.091g/cm³
LogP:3.17610

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of diethyl fluoro[4-(2-methylpropyl)phenyl]propanedioate

There total 3 articles about diethyl fluoro[4-(2-methylpropyl)phenyl]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 23197-72-0
diethyl (4-isobutylphenyl)propanedioate

: 23197-71-9
Fluor-<4-isobutyl-phenyl>-malonsaeure-diaethylester

Guidance literature:: diethyl (4-isobutylphenyl)propanedioate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

With Selectfluor; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jacs.1c12404

Reference yield:

: 15649-02-2
ethyl p-isobutylphenyl acetate

: 23197-71-9
Fluor-<4-isobutyl-phenyl>-malonsaeure-diaethylester

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With sodium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jacs.1c12404

Reference yield:

: 23197-71-9
Fluor-<4-isobutyl-phenyl>-malonsaeure-diaethylester

Guidance literature:: <4-Isobutyl-phenyl>-malonsaeure-diaethylester, 1) Natriumhydrid /Dimethylhydroformamid unter Stickstoff, 2) Rk.-Gemisch, FClO3, 0-10grad;

upstream raw materials:

ethyl p-isobutylphenyl acetate

diethyl (4-isobutylphenyl)propanedioate

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