(2E)-3-[4-(Dimethylamino)phenyl]-1-(2-hydroxyphenyl)prop-2-en-1-one

Base Information

• Chemical Name: (2E)-3-[4-(Dimethylamino)phenyl]-1-(2-hydroxyphenyl)prop-2-en-1-one
• CAS No.: 65786-13-2
• Molecular Formula: C17H17NO2
• Molecular Weight: 267.327
• Hs Code.: 2933599590

Synonyms:(2E)-3-[4-(DIMETHYLAMINO)PHENYL]-1-(2-HYDROXYPHENYL)PROP-2-EN-1-ONE;

Chemical Property of (2E)-3-[4-(Dimethylamino)phenyl]-1-(2-hydroxyphenyl)prop-2-en-1-one

Chemical Property:

• PSA: 40.54000
• LogP: 3.35430

Purity/Quality:

99% ^*data from raw suppliers

(2E)-3-[4-(Dimethylamino)phenyl]-1-(2-hydroxyphenyl)prop-2-en-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2E)-3-[4-(Dimethylamino)phenyl]-1-(2-hydroxyphenyl)prop-2-en-1-one

There total 8 articles about (2E)-3-[4-(Dimethylamino)phenyl]-1-(2-hydroxyphenyl)prop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

o-hydroxyacetophenone (118-93-4,104809-67-8) + 4-dimethylamino-benzaldehyde (100-10-7) → 2'-hydroxy-4-dimethylaminochalcone (65786-13-2,6342-97-8)

Guidance literature:

o-hydroxyacetophenone; With sodium hydroxide; In ethanol; water; at 0 - 5 ℃;

4-dimethylamino-benzaldehyde; In ethanol; water;

DOI:10.2174/1570180815666180209151516

Reference yield: 93.0%

o-hydroxyacetophenone (118-93-4,104809-67-8) + 4-dimethylamino-benzaldehyde (100-10-7) → (E)-3-(4-(dimethylamino)phenyl)-1-(2-hydroxyphenyl)prop-2-en-1-one (65786-13-2)

Guidance literature:

With potassium hydroxide; ethanol; for 0.0333333h; Microwave irradiation;

DOI:10.1016/S0960-894X(02)00553-X

Reference yield: 17.0%

o-hydroxyacetophenone (118-93-4,104809-67-8) + 4-dimethylamino-benzaldehyde (100-10-7) → 2'-hydroxy-4-dimethylaminochalcone (65786-13-2,6342-97-8) + 2-[4-(dimethylamino)phenyl]-2,3-dihydro-4H-chromen-4-one (77038-22-3)

Guidance literature:

With potassium carbonate; In ethanol; for 10h; Reflux;

DOI:10.1016/j.tetlet.2011.07.072

upstream raw materials:

o-hydroxyacetophenone

4-dimethylamino-benzaldehyde

2-[4-(dimethylamino)phenyl]-2,3-dihydro-4H-chromen-4-one

Downstream raw materials:

[4-(4-dimethylamino-phenyl)-3,4-dihydro-2H-pyrazol-3-yl]-(2-hydroxy-phenyl)-ketone

3-(2-hydroxyphenyl)-5-(4-dimethylaminophenyl)-4,5-dihydro-1H-pyrazole

3-(2-hydroxyphenyl)-5-(4-dimethylaminophenyl)-4,5-dihydro-1-toluenesulphonylpyrazole

Acetic acid 2-[5-(4-dimethylamino-phenyl)-1-(toluene-4-sulfonyl)-4,5-dihydro-1H-pyrazol-3-yl]-phenyl ester

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