2,2'-[[1,1'-Biphenyl]-2,2'-diylbis(oxy)]dianiline

Base Information

Chemical Name:2,2'-[[1,1'-Biphenyl]-2,2'-diylbis(oxy)]dianiline
CAS No.:65801-89-0
Molecular Formula:C24H20N2O2
Molecular Weight:368.435
Hs Code.:
DSSTox Substance ID:DTXSID60602024
Nikkaji Number:J2.156.407I
Wikidata:Q82498943

Synonyms:65801-89-0;SCHEMBL560389;2,2'-[[1,1'-Biphenyl]-2,2'-diylbis(oxy)]dianiline;DTXSID60602024;2,2'-bis(o-aminophenoxy)biphenyl

Suppliers and Price of 2,2'-[[1,1'-Biphenyl]-2,2'-diylbis(oxy)]dianiline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,2'-[[1,1'-Biphenyl]-2,2'-diylbis(oxy)]dianiline

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:368.152477885
Heavy Atom Count:28
Complexity:432

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C2=CC=CC=C2OC3=CC=CC=C3N)OC4=CC=CC=C4N

Technology Process of 2,2'-[[1,1'-Biphenyl]-2,2'-diylbis(oxy)]dianiline

There total 4 articles about 2,2'-[[1,1'-Biphenyl]-2,2'-diylbis(oxy)]dianiline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 65811-04-3
2,2'-bis-(2-nitrophenoxy)-biphenyl

: 65801-89-0
2,2'-bis-(2-aminophenoxy)-biphenyl

Guidance literature:: With sulfuric acid; hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; for 8h; under 2068.59 Torr;
DOI:10.1016/j.jorganchem.2005.03.034

Reference yield:

: 1806-29-7
2,2'-dihydroxybiphenyl

: 65801-89-0
2,2'-bis-(2-aminophenoxy)-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: 97.2 percent / potassium carbonate / tetrahydrofuran / 72 h / Heating

2: 99.6 percent / hydrogen; conc. sulfuric acid / Pd/C / tetrahydrofuran / 8 h / 20 °C / 2068.59 Torr

With sulfuric acid; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1016/j.jorganchem.2005.03.034

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 65801-89-0
2,2'-bis-(2-aminophenoxy)-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: 97.2 percent / potassium carbonate / tetrahydrofuran / 72 h / Heating

2: 99.6 percent / hydrogen; conc. sulfuric acid / Pd/C / tetrahydrofuran / 8 h / 20 °C / 2068.59 Torr

With sulfuric acid; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1016/j.jorganchem.2005.03.034