Technology Process of 5-Butyl-5-methyl-1-pyrroline 1-oxide
There total 5 articles about 5-Butyl-5-methyl-1-pyrroline 1-oxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium chloride; zinc;
In
ethanol; water;
for 12h;
Ambient temperature;
DOI:10.1021/jm00162a004
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 50 percent / sodium nitrite, phloroglucinol dihydrate, urea / dimethylformamide / 96 h / Ambient temperature
2: 35 percent / Triton B / tetrahydrofuran / 5 h / 0 °C
3: 76 percent / p-toluenesulfonic acid / benzene / 2 h / Heating
4: 81 percent / zinc dust, ammonium chloride / ethanol; H2O / 12 h / Ambient temperature
With
3,5-dihydroxyphenol; ammonium chloride; N-benzyl-trimethylammonium hydroxide; toluene-4-sulfonic acid; urea; zinc; sodium nitrite;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00162a004
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 35 percent / Triton B / tetrahydrofuran / 5 h / 0 °C
2: 76 percent / p-toluenesulfonic acid / benzene / 2 h / Heating
3: 81 percent / zinc dust, ammonium chloride / ethanol; H2O / 12 h / Ambient temperature
With
ammonium chloride; N-benzyl-trimethylammonium hydroxide; toluene-4-sulfonic acid; zinc;
In
tetrahydrofuran; ethanol; water; benzene;
DOI:10.1021/jm00162a004