Benzamide, N,N'-1,2-phenylenebis[2-(diphenylphosphino)-

Base Information

Chemical Name:Benzamide, N,N'-1,2-phenylenebis[2-(diphenylphosphino)-
CAS No.:659727-33-0
Molecular Formula:C44H34N2O2P2
Molecular Weight:684.714
Hs Code.:
DSSTox Substance ID:DTXSID30412632

Synonyms:659727-33-0;N,N'-(1,2-Phenylene)bis(2-(diphenylphosphino)benzamide);Benzamide, N,N'-1,2-phenylenebis[2-(diphenylphosphino)-;DTXSID30412632

Suppliers and Price of Benzamide, N,N'-1,2-phenylenebis[2-(diphenylphosphino)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzamide, N,N'-1,2-phenylenebis[2-(diphenylphosphino)-

Chemical Property:

XLogP3:9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:10
Exact Mass:684.20955233
Heavy Atom Count:50
Complexity:929

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(C2=CC=CC=C2)C3=CC=CC=C3C(=O)NC4=CC=CC=C4NC(=O)C5=CC=CC=C5P(C6=CC=CC=C6)C7=CC=CC=C7

Technology Process of Benzamide, N,N'-1,2-phenylenebis[2-(diphenylphosphino)-

There total 1 articles about Benzamide, N,N'-1,2-phenylenebis[2-(diphenylphosphino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.5%

: 17261-28-8
ortho-diphenylphosphinobenzoic acid

: 95-54-5
1,2-diamino-benzene

: 659727-33-0
1,2-Bis-N-[2'-(diphenylphosphanyl)benzoyl]diaminobenzene

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 14h;
DOI:10.1016/j.ica.2014.08.033

Reference yield: 79.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 659727-33-0
1,2-Bis-N-[2'-(diphenylphosphanyl)benzoyl]diaminobenzene

: 659727-34-1
[PdCl₂(1,2-bis-N[2'-diphenylphosphanyl)benzoyl]diaminobenzene]

Guidance literature:: In dichloromethane; byproducts: cod; all manipulations under N2 atm.; soln. of Pd and org. compds. allowed tostand at room temp. for 3 h; filtered, concd. in vac., chromy. (silica, CH2Cl2/EtOH (4:1)), solvent evapd., elem. anal.;
DOI:10.1002/ejic.200300360

Reference yield: 75.3%

: nickel(II) perchlorate hexahydrate

: 659727-33-0
1,2-Bis-N-[2'-(diphenylphosphanyl)benzoyl]diaminobenzene

: C₄₄H₃₂N₂NiO₂P₂

Guidance literature:: 1,2-Bis-N-[2'-(diphenylphosphanyl)benzoyl]diaminobenzene; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 45 ℃;

nickel(II) perchlorate hexahydrate; In N,N-dimethyl-formamide; for 3h;
DOI:10.1016/j.ica.2014.08.033