Thiazole, 2-methyl-4-phenyl-5-(tributylstannyl)-

Base Information

• Chemical Name: Thiazole, 2-methyl-4-phenyl-5-(tributylstannyl)-
• CAS No.: 660435-07-4
• Molecular Formula: C22H35NSSn
• Molecular Weight: 464.303
• Mol file: 660435-07-4.mol

Synonyms:

Chemical Property of Thiazole, 2-methyl-4-phenyl-5-(tributylstannyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Thiazole, 2-methyl-4-phenyl-5-(tributylstannyl)-

There total 1 articles about Thiazole, 2-methyl-4-phenyl-5-(tributylstannyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H8LiNS (50834-80-5) + tributyltin chloride (1461-22-9) → 2-methyl-4-phenyl-5-(tributylstannyl)thiazole (660435-07-4)

Guidance literature:

In tetrahydrofuran; at -78 - 20 ℃; for 2h;

Reference yield: 2.0%

2-methyl-4-phenyl-5-(tributylstannyl)thiazole (660435-07-4) + 6-iodo-1-(propane-2-sulfonyl)-1H-benzimidazole-2-ylamine (208335-92-6) → 1-isopropylsulfonyl-2-amino-6-(2-(methyl)-4-(phenyl)-thiazol-5-yl)-benzimidazole

Guidance literature:

dichloro bis(acetonitrile) palladium(II); In DMF (N,N-dimethyl-formamide); at 100 ℃; for 4h;

upstream raw materials:

C₁₀H₈LiNS

tributyltin chloride

Refernces