Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 3-[[[(1S)-2-(1,1-dimethylethoxy)-2-oxo-1-(phenylmethyl)ethyl]amino]carb onyl]-, methyl ester, (1R,2S,3R,4S)-

Base Information

Chemical Name:Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 3-[[[(1S)-2-(1,1-dimethylethoxy)-2-oxo-1-(phenylmethyl)ethyl]amino]carb onyl]-, methyl ester, (1R,2S,3R,4S)-
CAS No.:660439-16-7
Molecular Formula:C23H29NO5
Molecular Weight:399.487
Hs Code.:

Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid,
3-[[[(1S)-2-(1,1-dimethylethoxy)-2-oxo-1-(phenylmethyl)ethyl]amino]carb
onyl]-, methyl ester, (1R,2S,3R,4S)-

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Chemical Property of Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 3-[[[(1S)-2-(1,1-dimethylethoxy)-2-oxo-1-(phenylmethyl)ethyl]amino]carb onyl]-, methyl ester, (1R,2S,3R,4S)-

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Technology Process of Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 3-[[[(1S)-2-(1,1-dimethylethoxy)-2-oxo-1-(phenylmethyl)ethyl]amino]carb onyl]-, methyl ester, (1R,2S,3R,4S)-

There total 1 articles about Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 3-[[[(1S)-2-(1,1-dimethylethoxy)-2-oxo-1-(phenylmethyl)ethyl]amino]carb onyl]-, methyl ester, (1R,2S,3R,4S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 16874-17-2
L-phenylalanine tert-butyl ester

: 96243-74-2
(1S,2R,3S,4R)-3-(methoxycarbonyl)bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

: 660439-16-7
(2S,3R)-3-endo-(1-tert-butoxycarbonyl-2-phenyl-ethylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-endo-carboxylic acid methyl ester

Guidance literature:: With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 13h;
DOI:10.1021/jo030295+