AZO-TERT-OCTANE

Base Information

Chemical Name:AZO-TERT-OCTANE
CAS No.:39198-34-0
Molecular Formula:C16H34N2
Molecular Weight:254.459
Hs Code.:
Mol file:39198-34-0.mol

Synonyms:Diazene,bis(1,1,3,3-tetramethylbutyl)- (9CI);1,1,1',1',3,3,3',3'-Octamethyl-1,1'-azobutane;2,2'-Azobis(2,4,4-trimethylpentane);Azo-tert-octane;Di-tert-octyldiazene;VR 110;Bis(2,4,4-trimethylpentan-2-yl)diazene;

Suppliers and Price of AZO-TERT-OCTANE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
AZO-TERT-OCTANE 95.00%
5MG
$ 501.66

Total 50 raw suppliers

Chemical Property of AZO-TERT-OCTANE

Chemical Property:

Vapor Pressure:0.00314mmHg at 25°C
Refractive Index:1.442
Boiling Point:292.793 °C at 760 mmHg
Flash Point:122.776 °C
PSA：24.72000
Density:0.815 g/cm³
LogP:5.86820

Purity/Quality:

99%, ^*data from raw suppliers

AZO-TERT-OCTANE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of AZO-TERT-OCTANE

There total 6 articles about AZO-TERT-OCTANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 50780-12-6,40121-15-1
N,N'-bis(1,1,3,3-tetramethylbutyl)thiadiaziridine 1,1-dioxide

: 39198-34-0
N,N'-bis(1,1,3,3-tetramethylbutyl)diazene

Guidance literature:: With sodium hydroxide; In water; at 80 ℃; for 0.5h;
DOI:10.1021/jo00323a021

Reference yield:

: 6281-65-8
N,N'-bis(1,1,3,3-tetramethylbutyl)sulfamide

: 39198-34-0
N,N'-bis(1,1,3,3-tetramethylbutyl)diazene

Guidance literature:: Multistep reaction; (i) NaH, pentane, (ii) tBuOCl;
DOI:10.1055/s-1972-21965

Reference yield:

: 76613-31-5
N-chloro-N,N'-bis(1,1,3,3-tetramethylbutyl)sulfamide

: 39198-34-0
N,N'-bis(1,1,3,3-tetramethylbutyl)diazene

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / sodium hydride / tetrahydrofuran / 1.) -30 deg C, 2 h, 2.) 0 deg C, 1 h

2: 90 percent / 6 N NaOH / H₂O / 0.5 h / 80 °C / var. reaction partners, var. conditions

With sodium hydroxide; sodium hydride; In tetrahydrofuran; water;
DOI:10.1021/jo00323a021