(E)-5-[(1S,4aα)-Decahydro-5β-hydroxymethyl-5,8a-dimethyl-2-methylenenaphthalen-1β-yl]-3-methyl-2-pentenoic acid

Base Information

• Chemical Name: (E)-5-[(1S,4aα)-Decahydro-5β-hydroxymethyl-5,8a-dimethyl-2-methylenenaphthalen-1β-yl]-3-methyl-2-pentenoic acid
• CAS No.: 25671-16-3
• Molecular Formula: C₂₀H₃₂O₃
• Molecular Weight: 320.472
• Mol file: 25671-16-3.mol

Synonyms:2-Pentenoicacid, 5-[decahydro-5-(hydroxymethyl)-5,8a-dimethyl-2-methylene-1-naphthalenyl]-3-methyl-,[1S-[1a(E),4ab,5a,8aa]]-; Labda-8(20),13-dien-15-oicacid, 19-hydroxy- (7CI); Labda-8(20),13-dien-15-oic acid, 19-hydroxy-, (E)-(8CI); Agatholic acid

Chemical Property of (E)-5-[(1S,4aα)-Decahydro-5β-hydroxymethyl-5,8a-dimethyl-2-methylenenaphthalen-1β-yl]-3-methyl-2-pentenoic acid

Chemical Property:

• Boiling Point: 460.0±18.0 °C(Predicted)
• PKA: 5.16±0.33(Predicted)
• PSA: 57.53000
• Density: 1.06±0.1 g/cm3(Predicted)
• LogP: 4.56870

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (E)-5-[(1S,4aα)-Decahydro-5β-hydroxymethyl-5,8a-dimethyl-2-methylenenaphthalen-1β-yl]-3-methyl-2-pentenoic acid

There total 3 articles about (E)-5-[(1S,4aα)-Decahydro-5β-hydroxymethyl-5,8a-dimethyl-2-methylenenaphthalen-1β-yl]-3-methyl-2-pentenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetylagatholat → agatholic acid (25671-16-3)

Guidance literature:

With potassium hydroxide; In methanol;

DOI:10.1016/S0031-9422(00)91234-2

Reference yield:

→ agatholic acid (25671-16-3,28644-96-4,90527-79-0,126371-45-7,142434-37-5)

Guidance literature:

Methylester VIc, alkalische Hydrolyse;

Reference yield:

→ agatholic acid (25671-16-3)

Guidance literature:

Aus Agatholal u. AgNO3 in wss.-aethanol. NaOH;

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