5H-BENZOCYCLOHEPTENE-2,3,5-TRIOL, 6,7,8,9-TETRAHYDRO-6-AMINO-, cis-

Base Information

Chemical Name:5H-BENZOCYCLOHEPTENE-2,3,5-TRIOL, 6,7,8,9-TETRAHYDRO-6-AMINO-, cis-
CAS No.:58330-31-7
Molecular Formula:C11H15NO3
Molecular Weight:209.2417
Hs Code.:
DSSTox Substance ID:DTXSID10207063
Nikkaji Number:J220.772I
Wikidata:Q76003137
ChEMBL ID:CHEMBL319358

Synonyms:cis-6,7,8,9-Tetrahydro-6-amino-5H-benzocycloheptene-2,3,5-triol;5H-BENZOCYCLOHEPTENE-2,3,5-TRIOL, 6,7,8,9-TETRAHYDRO-6-AMINO-, cis-;cis-2,3-Dihydroxy-6-amino-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-ol;58330-31-7;CHEMBL319358;DTXSID10207063;LS-33894;6,7,8,9-Tetrahydro-6alpha-amino-5H-benzocycloheptene-2,3,5alpha-triol

Suppliers and Price of 5H-BENZOCYCLOHEPTENE-2,3,5-TRIOL, 6,7,8,9-TETRAHYDRO-6-AMINO-, cis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5H-BENZOCYCLOHEPTENE-2,3,5-TRIOL, 6,7,8,9-TETRAHYDRO-6-AMINO-, cis-

Chemical Property:

Vapor Pressure:5.02E-09mmHg at 25°C
Boiling Point:453.8°Cat760mmHg
Flash Point:228.3°C
Density:1.346g/cm³
XLogP3:0.2
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:209.10519334
Heavy Atom Count:15
Complexity:224

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(C(C2=CC(=C(C=C2C1)O)O)O)N
Isomeric SMILES:C1C[C@H]([C@H](C2=CC(=C(C=C2C1)O)O)O)N

Technology Process of 5H-BENZOCYCLOHEPTENE-2,3,5-TRIOL, 6,7,8,9-TETRAHYDRO-6-AMINO-, cis-

There total 5 articles about 5H-BENZOCYCLOHEPTENE-2,3,5-TRIOL, 6,7,8,9-TETRAHYDRO-6-AMINO-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945-53-9
2,3-dihydroxy-6,7,8,9-tetrahydro-5H-benzocycloheptenone

: 58330-31-7
cis-2,3-dihydroxy-6-amino-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-ol

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / acetone

2: nBuONO, HCl / diethyl ether

3: LiAlH₄ / tetrahydrofuran

4: H₂, AcOH / Pd-C

With hydrogenchloride; lithium aluminium tetrahydride; n-Butyl nitrite; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1021/jm00271a007

Reference yield:

: 951-99-5
2,3-dimethoxy-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

: 58330-31-7
cis-2,3-dihydroxy-6-amino-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-ol

Guidance literature:: Multi-step reaction with 5 steps

1: AlCl₃ / benzene

2: K₂CO₃ / acetone

3: nBuONO, HCl / diethyl ether

4: LiAlH₄ / tetrahydrofuran

5: H₂, AcOH / Pd-C

With hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; n-Butyl nitrite; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; acetone; benzene;
DOI:10.1021/jm00271a007

Reference yield:

: 35872-51-6
2,3-dibenzyloxy-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

: 58330-31-7
cis-2,3-dihydroxy-6-amino-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-ol

Guidance literature:: Multi-step reaction with 3 steps

1: nBuONO, HCl / diethyl ether

2: LiAlH₄ / tetrahydrofuran

3: H₂, AcOH / Pd-C

With hydrogenchloride; lithium aluminium tetrahydride; n-Butyl nitrite; hydrogen; acetic acid; palladium on activated charcoal; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00271a007