(3-Aminophenyl)phenylarsinic acid

Base Information

• Chemical Name: (3-Aminophenyl)phenylarsinic acid
• CAS No.: 7150-96-1
• Molecular Formula: C₁₂H₁₂AsNO₂
• Molecular Weight: 277.154
• NSC Number: 41378
• DSSTox Substance ID: DTXSID10285326
• Wikidata: Q82020659
• ChEMBL ID: CHEMBL1511311

Synonyms:MLS000737040;7150-96-1;(3-aminophenyl)phenylarsinic acid;NSC41378;ANTINEOPLASTIC-41378;CHEMBL1511311;DTXSID10285326;HMS2763F08;NSC-41378;SMR000393996

Chemical Property of (3-Aminophenyl)phenylarsinic acid

Chemical Property:

• Vapor Pressure: 1.17E-11mmHg at 25°C
• Boiling Point: 520.4°Cat760mmHg
• Flash Point: 268.6°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 277.008398
• Heavy Atom Count: 16
• Complexity: 276

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)[As](=O)(C2=CC=CC(=C2)N)O

Technology Process of (3-Aminophenyl)phenylarsinic acid

There total 2 articles about (3-Aminophenyl)phenylarsinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3-nitro-phenyl)-phenyl-arsinic acid (108880-49-5) → (3-amino-phenyl)-phenyl-arsinic acid (7150-96-1)

Guidance literature:

With sodium hydroxide; iron(II) hydroxide;

DOI:10.1021/ja01282a030

Reference yield:

3-nitro-aniline (99-09-2) → (3-amino-phenyl)-phenyl-arsinic acid (7150-96-1)

Guidance literature:

Multi-step reaction with 2 steps

1: water / Diazotization_.anschliessend mit Arsenosobenzol und wss. Natronlauge

2: iron (II)-hydroxide; aq. NaOH solution

With sodium hydroxide; iron(II) hydroxide; water;

DOI:10.1021/ja01282a030

Reference yield:

(3-amino-phenyl)-phenyl-arsinic acid (7150-96-1) → (3-hydroxy-phenyl)-phenyl-arsinic acid (857587-41-8)

Guidance literature:

With sulfuric acid; sodium nitrite;

DOI:10.1021/ja01282a030

upstream raw materials:

(3-nitro-phenyl)-phenyl-arsinic acid

3-nitro-aniline

Downstream raw materials:

(3-hydroxy-phenyl)-phenyl-arsinic acid

As,As'-bis-(3-hydroxy-phenyl)-As,As'-diphenyl-diarsane

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