Technology Process of 1-Methyl-2-(octyloxy)benzene
There total 4 articles about 1-Methyl-2-(octyloxy)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; caesium carbonate; sodium L-ascorbate;
In
dimethyl sulfoxide;
at 60 ℃;
for 12h;
Catalytic behavior;
Schlenk technique;
Molecular sieve;
Green chemistry;
DOI:10.1016/j.tet.2015.08.066
- Guidance literature:
-
2-methylphenyl bromide;
With
copper(l) iodide; 2-methyl-8-quinolinol; tetra(n-butyl)ammonium hydroxide;
In
water; dimethyl sulfoxide;
at 130 ℃;
1-bromo-octane;
With
tetra(n-butyl)ammonium hydroxide;
In
water; dimethyl sulfoxide;
at 100 ℃;
DOI:10.1055/s-0030-1258965
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: copper(ll) sulfate pentahydrate; water; potassium hydroxide; sodium L-ascorbate / dimethyl sulfoxide / 24 h / 120 °C / Schlenk technique; Green chemistry
1.2: 0.5 h / 20 °C / pH 2 - 3 / Schlenk technique; Green chemistry
2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate; caesium carbonate / dimethyl sulfoxide / 12 h / 60 °C / Schlenk technique; Molecular sieve; Green chemistry
With
copper(ll) sulfate pentahydrate; water; caesium carbonate; sodium L-ascorbate; potassium hydroxide;
In
dimethyl sulfoxide;
DOI:10.1016/j.tet.2015.08.066
