1-(Ethynylsulfanyl)-4-methylbenzene

Base Information

Chemical Name:1-(Ethynylsulfanyl)-4-methylbenzene
CAS No.:66823-38-9
Molecular Formula:C9H8S
Molecular Weight:148.229
Hs Code.:
DSSTox Substance ID:DTXSID30517055
Nikkaji Number:J2.062.778F
Wikidata:Q82378790

Synonyms:66823-38-9;1-(Ethynylsulfanyl)-4-methylbenzene;DTXSID30517055

Suppliers and Price of 1-(Ethynylsulfanyl)-4-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-(Ethynylsulfanyl)-4-methylbenzene

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:148.03467143
Heavy Atom Count:10
Complexity:134

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)SC#C

Technology Process of 1-(Ethynylsulfanyl)-4-methylbenzene

There total 12 articles about 1-(Ethynylsulfanyl)-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 88388-92-5
(4-Methylphenyl)(trichlorvinyl)thioether

: 66823-38-9
1-ethynylsulfanyl-4-methyl-benzene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; for 2h; Ambient temperature;

Reference yield: 32.0%

: 4-methylphenyl trimethylsilylethynyl sulfide

: 66823-38-9
1-ethynylsulfanyl-4-methyl-benzene

Guidance literature:: With potassium carbonate; In methanol; at 25 ℃; for 3h; Inert atmosphere;
DOI:10.1246/CL.200400

Reference yield:

: 106-45-6
para-thiocresol

: 66823-38-9
1-ethynylsulfanyl-4-methyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: EtONa / ethanol / Heating

2: 92 percent / LDA / diethyl ether / -78 - 0 °C

With sodium ethanolate; lithium diisopropyl amide; In diethyl ether; ethanol;
DOI:10.1021/jo0110146