6-Methyl-1,3-diazaspiro[4.5]decane-2,4-dione

Base Information

• Chemical Name: 6-Methyl-1,3-diazaspiro[4.5]decane-2,4-dione
• CAS No.: 707-15-3
• Molecular Formula: C₉H₁₄N₂O₂
• Molecular Weight: 182.222
• Hs Code.: 2933990090
• NSC Number: 38741,19566
• Mol file: 707-15-3.mol

Synonyms:6-Methyl-1,3-diazaspiro[4.5]decane-2,4-dione;707-15-3;NSC38741;6-Methyl-1,3-diazaspiro(4.5)decane-2,4-dione;6-methyl-1,3-diaza-spiro[4.5]decane-2,4-dione;10-methyl-2,4-diazaspiro[4.5]decane-1,3-dione;NIOSH/HM2784000;NSC19566;NSC-19566;NSC-38741;AKOS000263205;AKOS017268945;CS-0219563;HM27840000;EN300-04339;1,3-Diazaspiro(4.5)decane-2,4-dione, 6-methyl-;Z56862732;F1967-0973

Chemical Property of 6-Methyl-1,3-diazaspiro[4.5]decane-2,4-dione

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 58.20000
• Density: 1.2g/cm³
• LogP: 1.43230
• XLogP3: 1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 182.105527694
• Heavy Atom Count: 13
• Complexity: 264

Purity/Quality:

99% ^*data from raw suppliers

6-METHYL-1,3-DIAZA-SPIRO[4.5]DECANE-2,4-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CCCCC12C(=O)NC(=O)N2

Technology Process of 6-Methyl-1,3-diazaspiro[4.5]decane-2,4-dione

There total 6 articles about 6-Methyl-1,3-diazaspiro[4.5]decane-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

potassium cyanide + ammonium carbonate (506-87-6,6721-33-1,10361-29-2) + 2-Methylcyclohexanone (583-60-8) → 6-methyl-1,3-diazaspiro[4.5]decane-2,4-dione (707-15-3,83344-93-8,83344-94-9)

Guidance literature:

In ethanol; water; at 55 - 60 ℃;

DOI:10.1007/s00706-011-0600-9

Reference yield: 77.0%

potassium cyanide + 2-Methylcyclohexanone (583-60-8) → 6-methyl-1,3-diazaspiro[4.5]decane-2,4-dione (707-15-3,83344-93-8,83344-94-9)

Guidance literature:

With ammonium carbonate; In methanol; water; at 120 ℃; for 0.133333h; Sealed vial; Microwave irradiation;

DOI:10.3998/ark.5550190.0012.221

Reference yield:

sodium cyanide (143-33-9,25596-52-5) + 2-Methylcyclohexanone (583-60-8) → 2-methylcyclohexane-1-spiro-5'-hydantoin (707-15-3,83344-93-8,83344-94-9)

Guidance literature:

With ammonium carbonate;

DOI:10.1021/ja01255a014

upstream raw materials:

sodium cyanide

2-Methylcyclohexanone

potassium cyanide

ammonium carbonate

Downstream raw materials:

1-amino-2-methylcyclohexanecarboxylic acid

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