(1s,5s)-9-azabicyclo[3.3.1]nonane hydrochloride

Base Information

• Chemical Name: (1s,5s)-9-azabicyclo[3.3.1]nonane hydrochloride
• CAS No.: 6760-43-6
• Molecular Formula: C8H15N.ClH
• Molecular Weight: 161.675
• Hs Code.: 2933990090
• Mol file: 6760-43-6.mol

Synonyms:

Chemical Property of (1s,5s)-9-azabicyclo[3.3.1]nonane hydrochloride

Chemical Property:

• PSA: 12.03000
• LogP: 2.81180
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

9-azabicyclo[3.3.1]nonanehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1s,5s)-9-azabicyclo[3.3.1]nonane hydrochloride

There total 2 articles about (1s,5s)-9-azabicyclo[3.3.1]nonane hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-methyl-9-aza-bicyclo[3.3.1]nonane (491-25-8) → 9-azabicyclo<3.3.1>nonane hydrochloride (6760-43-6)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: MeOH

With methanol; triethylamine; In dichloromethane;

DOI:10.1016/j.bmcl.2004.05.074

Reference yield:

9-(1-chloro-ethoxycarbonyl)-9-methyl-9-azonia-bicyclo[3.3.1]nonane; chloride → 9-azabicyclo<3.3.1>nonane hydrochloride (6760-43-6)

Guidance literature:

With methanol;

DOI:10.1016/j.bmcl.2004.05.074

Reference yield: 75.0%

C11H7BrF7NO + 9-azabicyclo<3.3.1>nonane hydrochloride (6760-43-6) → C19H21F7N2O

Guidance literature:

With potassium carbonate; sodium iodide; In acetonitrile; at 60 ℃; for 18h; Sealed tube;

DOI:10.1021/jacs.8b02142

upstream raw materials:

9-methyl-9-aza-bicyclo[3.3.1]nonane

Downstream raw materials:

9-propyl-9-azabicyclo<3.3.1>nonane

9-Isopropylazabicyclo<3.3.1>nonan

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