Trisodium 4-amino-3-[(e)-{4'-[(e)-(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3,3'-dimethylbiphenyl-4-yl}diazenyl]naphthalene-1,7-disulfonate

Base Information

Chemical Name:Trisodium 4-amino-3-[(e)-{4'-[(e)-(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3,3'-dimethylbiphenyl-4-yl}diazenyl]naphthalene-1,7-disulfonate
CAS No.:67617-63-4
Molecular Formula:C12H17NO2
Molecular Weight:207.272
Hs Code.:
DSSTox Substance ID:DTXSID2070265,DTXSID20275995
Nikkaji Number:J453.323B

Trisodium 4-amino-3-[(e)-{4'-[(e)-(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3,3'-dimethylbiphenyl-4-yl}diazenyl]naphthalene-1,7-disulfonate

Synonyms:65152-15-0;1,7-Naphthalenedisulfonic acid, 4-amino-3-[[4'-[(1-amino-4-sulfo-2-naphthalenyl)azo]-3,3'-dimethyl[1,1'-biphenyl]-4-yl]azo]-, trisodium salt;1,7-Naphthalenedisulfonic acid, 4-amino-3-((4'-((1-amino-4-sulfo-2-naphthalenyl)azo)-3,3'-dimethyl(1,1'-biphenyl)-4-yl)azo)-, trisodium salt;trisodium 4-amino-3-[(e)-{4'-[(e)-(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3,3'-dimethylbiphenyl-4-yl}diazenyl]naphthalene-1,7-disulfonate;67617-63-4;DTXSID2070265;DTXSID20275995;1,7-Naphthalenedisulfonic acid, 4-amino-3-((4'-((1-amino-4-sulfo-2-naphthyl)azo)-3,3'-dimethyl-4-biphenylyl)azo)-, trisodium salt;1,7-Naphthalenedisulfonic acid, 4-amino-3-(2-(4'-(2-(1-amino-4-sulfo-2-naphthalenyl)diazenyl)-3,3'-dimethyl(1,1'-biphenyl)-4-yl)diazenyl)-, sodium salt (1:3)

Suppliers and Price of Trisodium 4-amino-3-[(e)-{4'-[(e)-(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3,3'-dimethylbiphenyl-4-yl}diazenyl]naphthalene-1,7-disulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of Trisodium 4-amino-3-[(e)-{4'-[(e)-(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3,3'-dimethylbiphenyl-4-yl}diazenyl]naphthalene-1,7-disulfonate

Chemical Property:

Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:15
Rotatable Bond Count:5
Exact Mass:826.05382276
Heavy Atom Count:55
Complexity:1610

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1)C2=CC(=C(C=C2)N=NC3=C(C4=CC=CC=C4C(=C3)S(=O)(=O)[O-])N)C)N=NC5=CC(=C6C=C(C=CC6=C5N)S(=O)(=O)[O-])S(=O)(=O)[O-].[Na+].[Na+].[Na+]

Technology Process of Trisodium 4-amino-3-[(e)-{4'-[(e)-(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3,3'-dimethylbiphenyl-4-yl}diazenyl]naphthalene-1,7-disulfonate

There total 8 articles about Trisodium 4-amino-3-[(e)-{4'-[(e)-(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3,3'-dimethylbiphenyl-4-yl}diazenyl]naphthalene-1,7-disulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71626-44-3
methyl 2-(2,6-dimethylphenylimino)propanoate

: 57646-33-0
methyl (2R)-2-[(2,6-dimethylphenyl)amino]propanoate

: 67617-63-4
(S)-methyl 2-(2,6-dimethylphenylamino)propanoate

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₉H₃₄FeN₂P₂; hydrogen; In 1,2-dichloro-ethane; at 80 ℃; for 3h; under 37503.8 Torr; Overall yield = 96 percent; enantioselective reaction; Autoclave;

Reference yield:

: 5445-17-0
Methyl 2-bromopropionate

: 87-62-7
2,6-dimethylaniline

: 67617-63-4
(S)-methyl 2-(2,6-dimethylphenylamino)propanoate

Guidance literature:: With sodium hydrogencarbonate; In ice-water; nitrogen;

Reference yield:

: 52888-49-0
methyl N-(2,6-dimethylphenyl)alaninate

: 67617-63-4
(S)-methyl 2-(2,6-dimethylphenylamino)propanoate

: 57646-32-9,83234-64-4
(2R)-2-[(2,6-dimethylphenyl)amino]propanoic acid

Guidance literature:: With phosphate buffer; Burkholderia cepacia lipase PS; Triton X-100; In water; at 30 ℃; for 24h; pH=7.0;
DOI:10.1016/j.tetasy.2005.01.033