Benzoic acid, 2-chloro-3,4-bis(phenylmethoxy)-

Base Information

Chemical Name:Benzoic acid, 2-chloro-3,4-bis(phenylmethoxy)-
CAS No.:67632-03-5
Molecular Formula:C21H17ClO4
Molecular Weight:368.817
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid, 2-chloro-3,4-bis(phenylmethoxy)-

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Technology Process of Benzoic acid, 2-chloro-3,4-bis(phenylmethoxy)-

There total 3 articles about Benzoic acid, 2-chloro-3,4-bis(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

: 37687-59-5
3,4-dibenzyloxy-2-chlorobenzaldehyde

: 67632-03-5
3,4-bis(benzyloxy)-2-chlorobenzoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; In N,N-dimethyl-formamide; at 30 ℃; for 3h; Inert atmosphere;

Reference yield:

: 5417-17-4
2-chloro-3,4-dimethoxybenzaldehyde

: 67632-03-5
3,4-bis(benzyloxy)-2-chlorobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride; pyridine / N,N-dimethyl acetamide / 5 h / 55 °C / Inert atmosphere; Reflux

2: sodium carbonate; sodium iodide / N,N-dimethyl-formamide / 2 h / 40 °C / Inert atmosphere

3: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / N,N-dimethyl-formamide / 3 h / 30 °C / Inert atmosphere

With pyridine; aluminum (III) chloride; sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; sodium carbonate; sodium iodide; In N,N-dimethyl acetamide; N,N-dimethyl-formamide;

Reference yield:

: 32864-11-2
2-Chloro-3,4-dihydroxybenzaldehyde

: 67632-03-5
3,4-bis(benzyloxy)-2-chlorobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; sodium iodide / N,N-dimethyl-formamide / 2 h / 40 °C / Inert atmosphere

2: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / N,N-dimethyl-formamide / 3 h / 30 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; sodium carbonate; sodium iodide; In N,N-dimethyl-formamide;