1-Bromo-6-nitronaphthalene

Base Information

• Chemical Name: 1-Bromo-6-nitronaphthalene
• CAS No.: 67878-75-5
• Molecular Formula: C10H6BrNO2
• Molecular Weight: 252.06400
• DSSTox Substance ID: DTXSID80704751
• Nikkaji Number: J150.665J
• Wikidata: Q82637279
• Mol file: 67878-75-5.mol

Synonyms:1-Bromo-6-nitronaphthalene;67878-75-5;Naphthalene, 1-bromo-6-nitro-;SCHEMBL8489789;DTXSID80704751;FT-0728314

Chemical Property of 1-Bromo-6-nitronaphthalene

Chemical Property:

• Melting Point: 130-131 °C
• Boiling Point: 375.0±15.0 °C(Predicted)
• PSA: 45.82000
• Density: 1.662±0.06 g/cm3(Predicted)
• LogP: 4.03370
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 250.95819
• Heavy Atom Count: 14
• Complexity: 229

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC2=C(C=CC(=C2)[N+](=O)[O-])C(=C1)Br

Technology Process of 1-Bromo-6-nitronaphthalene

There total 8 articles about 1-Bromo-6-nitronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-6-nitro-[2]naphthylamine (843668-15-5) → 1-bromo-6-nitro-naphthalene (67878-75-5)

Guidance literature:

With sulfuric acid; acetic acid; Diazotization_.Behandlung der Diazoniumsalz-Loesung mit Cu₂O in Methanol;

DOI:10.1017/S0317167100001372 DOI:10.1039/jr9430000391

Reference yield:

2-nitronaphthalene (581-89-5) → 1-bromo-6-nitro-naphthalene (67878-75-5)

Guidance literature:

With bromine;

Reference yield:

6-nitro-1-naphthylamine (3229-88-7) → 1-bromo-6-nitro-naphthalene (67878-75-5)

Guidance literature:

With hydrogen bromide; Diazotization_.Erwaermen der Diazoniumsalz-Loesung mit CuBr in wss. HBr auf 60grad;

DOI:10.1039/jr9430000391

upstream raw materials:

2-nitronaphthalene

1-bromo-6-nitro-[2]naphthylamine

6-nitro-1-naphthylamine

bromine

Downstream raw materials:

6-amino-1-bromonaphthalene