2,2'-{Methylenebis[(2-hydroxy-3,1-phenylene)methylene]}diphenol

Base Information

Chemical Name:2,2'-{Methylenebis[(2-hydroxy-3,1-phenylene)methylene]}diphenol
CAS No.:67988-30-1
Molecular Formula:C27H24O4
Molecular Weight:412.485
Hs Code.:
DSSTox Substance ID:DTXSID70559333
Nikkaji Number:J1.095.731A
Wikidata:Q82442017

Synonyms:67988-30-1;SCHEMBL5852506;DTXSID70559333;2,2'-{Methylenebis[(2-hydroxy-3,1-phenylene)methylene]}diphenol

Suppliers and Price of 2,2'-{Methylenebis[(2-hydroxy-3,1-phenylene)methylene]}diphenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,2'-{Methylenebis[(2-hydroxy-3,1-phenylene)methylene]}diphenol

Chemical Property:

XLogP3:6.3
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:412.16745924
Heavy Atom Count:31
Complexity:493

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CC2=C(C(=CC=C2)CC3=CC=CC(=C3O)CC4=CC=CC=C4O)O)O

Technology Process of 2,2'-{Methylenebis[(2-hydroxy-3,1-phenylene)methylene]}diphenol

There total 9 articles about 2,2'-{Methylenebis[(2-hydroxy-3,1-phenylene)methylene]}diphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 992-52-9
2-<3-<3-(5-tert-Butylsalicyl)-5-tert-butylsalicyl>-5-tert-butylsalicyl>-4-tert-butylphenol

: 67988-30-1
2,2'-methylenebis<6-(2-hydroxybenzyl)phenol>

Guidance literature:: With aluminium trichloride; In toluene; at 50 ℃; for 2h;
DOI:10.1246/bcsj.62.1111

Reference yield:

: 98-54-4
para-tert-butylphenol

: 67988-30-1
2,2'-methylenebis<6-(2-hydroxybenzyl)phenol>

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / p-toluenesulfonic acid / benzene / 24 h / Heating

2: 65 percent / AlCl₃ / toluene / 2 h / 50 °C

With aluminium trichloride; toluene-4-sulfonic acid; In toluene; benzene;
DOI:10.1246/bcsj.62.1111

Reference yield:

: 810-52-6
4-(tert-butyl)-2,6-bis{[5-(tert-butyl)-2-hydroxyphenyl]methyl}phenol

: 67988-30-1
2,2'-methylenebis<6-(2-hydroxybenzyl)phenol>

Guidance literature:: Multi-step reaction with 3 steps

1: 34 percent / 10percent aq. NaOH / methanol / 35 h / 60 °C

2: 64 percent / p-toluenesulfonic acid / benzene / 24 h / Heating

3: 65 percent / AlCl₃ / toluene / 2 h / 50 °C

With sodium hydroxide; aluminium trichloride; toluene-4-sulfonic acid; In methanol; toluene; benzene;
DOI:10.1246/bcsj.62.1111