1,1'-[Oxybis(methylene)]bis(3,4,5-trimethoxybenzene)

Base Information

Chemical Name:1,1'-[Oxybis(methylene)]bis(3,4,5-trimethoxybenzene)
CAS No.:68299-87-6
Molecular Formula:C20H26O7
Molecular Weight:378.422
Hs Code.:
DSSTox Substance ID:DTXSID50576124
Nikkaji Number:J1.050.621B
Wikidata:Q82465672

Synonyms:68299-87-6;3,4,5-tri-methoxybenzyloxide;SCHEMBL7961363;DTXSID50576124;1,1'-[Oxybis(methylene)]bis(3,4,5-trimethoxybenzene)

Suppliers and Price of 1,1'-[Oxybis(methylene)]bis(3,4,5-trimethoxybenzene)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,1'-[Oxybis(methylene)]bis(3,4,5-trimethoxybenzene)

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:10
Exact Mass:378.16785316
Heavy Atom Count:27
Complexity:344

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1OC)OC)COCC2=CC(=C(C(=C2)OC)OC)OC

Technology Process of 1,1'-[Oxybis(methylene)]bis(3,4,5-trimethoxybenzene)

There total 4 articles about 1,1'-[Oxybis(methylene)]bis(3,4,5-trimethoxybenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 61165-98-8
1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene

: 68299-87-6
5,5'-(oxybis(methylene))bis(1,2,3-trimethoxybenzene)

: <2'(3'',4'',5''-trimethoxybenzyl)(3',4',5'-trimethoxybenzyl)3,4,5-trimethoxybenzyl> ether

: 2'<2'',(3''',4''',5'''-trimethoxybenzyl)3'',4'',5''-trimethoxybenzyl>3',4',5'-trimethoxybenzyl ether

Guidance literature:: In carbon disulfide; for 7h; Heating; in presence of bentonite-clay;
DOI:10.1016/S0040-4039(00)78187-1

Reference yield: 6.0%

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 68299-87-6
5,5'-(oxybis(methylene))bis(1,2,3-trimethoxybenzene)

Guidance literature:: With proton exchanged montmorillonite; In dichloromethane; at 25 ℃;
DOI:10.1016/j.tetlet.2020.152584

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 68299-87-6
5,5'-(oxybis(methylene))bis(1,2,3-trimethoxybenzene)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 20 °C

2: proton exchanged montmorillonite / dichloromethane / 25 °C

With sodium tetrahydroborate; In ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2020.152584