3-nitrophenyl azide

Base Information

• Chemical Name: 3-nitrophenyl azide
• CAS No.: 1516-59-2
• Molecular Formula: C6H4 N4 O2
• Molecular Weight: 164.123
• Hs Code.: 2929909090
• Mol file: 1516-59-2.mol

Synonyms:1-Azido-3-nitrobenzene;3-Nitrophenyl azide; m-Nitrophenyl azide

Chemical Property of 3-nitrophenyl azide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 95.57000
• Density: g/cm³
• LogP: 2.51256

Purity/Quality:

99% ^*data from raw suppliers

1-azido-3-nitrobenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-nitrophenyl azide

There total 35 articles about 3-nitrophenyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-nitro-aniline (99-09-2) → 3-nitrophenyl azide (1516-59-2)

Guidance literature:

3-nitro-aniline; With hydrogenchloride; sodium nitrite; In water; for 0.5h; Cooling with ice;

With sodium azide; In water; at 20 ℃; for 2h; Cooling with ice;

DOI:10.1016/j.steroids.2019.108431

Reference yield: 95.0%

4,4,5,5-tetramethyl-2-(3-nitrophenyl)-1,3,2-dioxaborolane (68716-48-3) → 3-nitrophenyl azide (1516-59-2)

Guidance literature:

With trimethylsilylazide; tetrabutyl ammonium fluoride; copper(l) chloride; In tetrahydrofuran; methanol; for 8h; Reflux; In air;

DOI:10.1002/chem.201000971

Reference yield: 93.0%

m-nitrobenzene boronic acid (13331-27-6) → 3-nitrophenyl azide (1516-59-2)

Guidance literature:

With trimethylsilylazide; tetrabutyl ammonium fluoride; copper(l) chloride; In tetrahydrofuran; methanol; for 4.5h; Reflux; In air;

DOI:10.1002/chem.201000971

upstream raw materials:

1-nitro-3-nitrosobenzene

3-nitro-aniline

3-nitrophenyldiazonium tetrafluoroborate

3-nitrophenylhydrazine

Downstream raw materials:

1-(3-Nitro-phenyl)-1H-[1,2,3]triazole-4-carbonitrile

[3,4-Di-tert-butyl-1-(2,4,6-trimethyl-phenyl)-1H-phosphet-(2Z)-ylidene]-(3-nitro-phenyl)-amine

(E)-1,2-bis(3-nitrophenyl)diazene

2-(diethylamino)-4-nitro-3H-azepine

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