Technology Process of 6H-Cyclopenta(ghi)picene
There total 8 articles about 6H-Cyclopenta(ghi)picene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: AlCl3 / CH2Cl2 / 16 h / 5 °C
2: hydrazine, KOH / bis-(2-hydroxy-ethyl) ether / 18 h / Heating
3: methanesulfonic acid
4: 93 percent / 10percent Pd/C / various solvent(s) / Heating
5: KOH / ethanol / 5 h / Heating
6: liquid HF
7: NaBH4 / ethanol
8: 10percent Pd/C / various solvent(s) / 18 h / Heating
With
potassium hydroxide; sodium tetrahydroborate; aluminium trichloride; methanesulfonic acid; hydrazine;
palladium on activated charcoal;
In
ethanol; dichloromethane; hydrogen fluoride; diethylene glycol;
DOI:10.1021/jo00067a065
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaBH4 / ethanol
2: 10percent Pd/C / various solvent(s) / 18 h / Heating
With
sodium tetrahydroborate;
palladium on activated charcoal;
In
ethanol;
DOI:10.1021/jo00067a065
- Guidance literature:
-
Multi-step reaction with 3 steps
1: liquid HF
2: NaBH4 / ethanol
3: 10percent Pd/C / various solvent(s) / 18 h / Heating
With
sodium tetrahydroborate;
palladium on activated charcoal;
In
ethanol; hydrogen fluoride;
DOI:10.1021/jo00067a065