Benzoic acid, 4-[2-[5-chloro-2-[2-[[[(2,4-dichlorophenyl)methyl]sulfonyl]amino]ethyl]-1-( diphenylmethyl)-1H-indol-3-yl]ethoxy]-, methyl ester

Base Information

Chemical Name:Benzoic acid, 4-[2-[5-chloro-2-[2-[[[(2,4-dichlorophenyl)methyl]sulfonyl]amino]ethyl]-1-( diphenylmethyl)-1H-indol-3-yl]ethoxy]-, methyl ester
CAS No.:683813-13-0
Molecular Formula:C40H35Cl3N2O5S
Molecular Weight:762.153
Hs Code.:

Benzoic acid,
4-[2-[5-chloro-2-[2-[[[(2,4-dichlorophenyl)methyl]sulfonyl]amino]ethyl]-1-(
diphenylmethyl)-1H-indol-3-yl]ethoxy]-, methyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-[2-[5-chloro-2-[2-[[[(2,4-dichlorophenyl)methyl]sulfonyl]amino]ethyl]-1-( diphenylmethyl)-1H-indol-3-yl]ethoxy]-, methyl ester

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Technology Process of Benzoic acid, 4-[2-[5-chloro-2-[2-[[[(2,4-dichlorophenyl)methyl]sulfonyl]amino]ethyl]-1-( diphenylmethyl)-1H-indol-3-yl]ethoxy]-, methyl ester

There total 6 articles about Benzoic acid, 4-[2-[5-chloro-2-[2-[[[(2,4-dichlorophenyl)methyl]sulfonyl]amino]ethyl]-1-( diphenylmethyl)-1H-indol-3-yl]ethoxy]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 540522-69-8
methyl 4-{2-[2-(2-aminoethyl)-1-benzhydryl-5-chloro-1H-indol-3-yl]ethoxy}benzoate amine

: 88691-50-3
(2,4-dichlorophenyl)methanesulfonyl chloride

: 683813-13-0
methyl 4-{2-[5-chloro-2-(2-{[(2,4-dichlorobenzyl)sulfonyl]amino}ethyl)-1-(diphenylmethyl)-1H-indol-3-yl]ethoxy}benzoate

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane;
DOI:10.1021/jm061131z

Reference yield: 98.0%

: 683813-13-0
methyl 4-{2-[5-chloro-2-(2-{[(2,4-dichlorobenzyl)sulfonyl]amino}ethyl)-1-(diphenylmethyl)-1H-indol-3-yl]ethoxy}benzoate

Guidance literature:

Reference yield:

: 479422-24-7
methyl 4-[2-[5-chloro-(1-diphenylmethyl)-2-methyl-1H-indol-3-yl]ethoxy]benzoate

: 683813-13-0
methyl 4-{2-[5-chloro-2-(2-{[(2,4-dichlorobenzyl)sulfonyl]amino}ethyl)-1-(diphenylmethyl)-1H-indol-3-yl]ethoxy}benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: NBS; benzoyl peroxide / CCl₄ / 2.5 h / Heating

2: 0.750 g / Ag₂CO₃; H₂O / acetone

3: 23 percent / NH₄OAc / 4 h / Heating

4: 65 percent / Zn(Hg); aq. HCl / tetrahydrofuran / 1 h

5: 98 percent / aq. NaHCO₃ / CH₂Cl₂

With hydrogenchloride; N-Bromosuccinimide; ammonium acetate; water; sodium hydrogencarbonate; silver carbonate; mercury; zinc; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; dichloromethane; acetone; 3: Henry reaction / 5: Schotten-Baumann reaction;
DOI:10.1021/jm061131z