Ethyl 2-(2-(1,3-dioxolan-2-yl)ethyl)-3-oxobutanoate

Base Information

• Chemical Name: Ethyl 2-(2-(1,3-dioxolan-2-yl)ethyl)-3-oxobutanoate
• CAS No.: 24213-02-3
• Molecular Formula: C11H18 O5
• Molecular Weight: 230.261
• NSC Number: 79673,70306
• Mol file: 24213-02-3.mol

Synonyms:24213-02-3;Ethyl 2-(2-(1,3-dioxolan-2-yl)ethyl)-3-oxobutanoate;NSC70306;NSC 70306;ethyl 2-[2-(1,3-dioxolan-2-yl)ethyl]-3-oxobutanoate;NCIOpen2_003237;NCIOpen2_004332;SCHEMBL13243290;NSC79673;NSC-70306;NSC-79673;ethyl 2-[2-(1,3-dioxolan-2-yl)ethyl]-3-oxo-butanoate

Chemical Property of Ethyl 2-(2-(1,3-dioxolan-2-yl)ethyl)-3-oxobutanoate

Chemical Property:

• Vapor Pressure: 0.000656mmHg at 25°C
• Boiling Point: 309°Cat760mmHg
• Flash Point: 145.8°C
• Density: 1.104g/cm³
• XLogP3: 0.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 7
• Exact Mass: 230.11542367
• Heavy Atom Count: 16
• Complexity: 245

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)C(CCC1OCCO1)C(=O)C

Technology Process of Ethyl 2-(2-(1,3-dioxolan-2-yl)ethyl)-3-oxobutanoate

There total 2 articles about Ethyl 2-(2-(1,3-dioxolan-2-yl)ethyl)-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

2-bromo-2-(2-ethyl)dioxolane (18742-02-4) + ethyl acetoacetate (141-97-9) → 1-<2'-(1',3'-Dioxolanyl)>-3-carboethoxypentan-4-one (24213-02-3)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 18h; Heating;

DOI:10.1016/S0040-4039(01)00617-7

Reference yield:

→ 1-<2'-(1',3'-Dioxolanyl)>-3-carboethoxypentan-4-one (24213-02-3)

Guidance literature:

5-Oxo-2-acetyl-pentansaeure-ethylester, HO-CH2-CH2-OH, p-Toluolsulfonsaeure;

DOI:10.1021/jm00342a008

Reference yield: 51.0%

[3-(tert-butyl-dimethyl-silanyl)-1-ethynyl-prop-2-ynylidene]-(4-methoxy-phenyl)-amine + 1-<2'-(1',3'-Dioxolanyl)>-3-carboethoxypentan-4-one (24213-02-3) → 5-acetyl-6-[(tert-butyl-dimethyl-silanyl)-ethynyl]-3-(2-[1,3]dioxolan-2-yl-ethyl)-1-(4-methoxy-phenyl)-1H-pyridin-2-one

Guidance literature:

With sodium ethanolate; In 1,4-dioxane; for 5.5h; Heating;

DOI:10.3987/com-06-s(o)4

upstream raw materials:

2-bromo-2-(2-ethyl)dioxolane

ethyl acetoacetate

Downstream raw materials:

4-Hydroxy-2-mercapto-5-(2-<1,3-dioxolanyl-(2)>-ethyl)-6-methyl-pyrimidin

5-oxohexanal

4-Hydroxy-5-(2-<1,3-dioxolanyl-(2)>-ethyl)-6-methyl-pyrimidin

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