2,2-DIPHENYLACETOHYDRAZIDE

Base Information

• Chemical Name: 2,2-DIPHENYLACETOHYDRAZIDE
• CAS No.: 6636-02-8
• Molecular Formula: C14H14 N2 O
• Molecular Weight: 226.278
• Hs Code.: 2928000090
• Mol file: 6636-02-8.mol

Synonyms:Aceticacid, diphenyl-, hydrazide (6CI,8CI); 2,2-Diphenylacetohydrazide;Diphenylacetic acid hydrazide; Diphenylacetic hydrazide;Diphenylacetohydrazide; NSC 16288

Chemical Property of 2,2-DIPHENYLACETOHYDRAZIDE

Chemical Property:

• Vapor Pressure: 2.82E-08mmHg at 25°C
• Boiling Point: 449.6°C at 760 mmHg
• Flash Point: 225.7°C
• PSA: 55.12000
• Density: 1.156g/cm³
• LogP: 2.89960

Purity/Quality:

99% ^*data from raw suppliers

2,2-Diphenylacetohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2-DIPHENYLACETOHYDRAZIDE

There total 10 articles about 2,2-DIPHENYLACETOHYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methyl 2,2-diphenylacetate (3469-00-9) → diphenylacetylhydrazine (6636-02-8)

Guidance literature:

With hydrazine hydrate; In ethanol; for 1h; Reflux;

Reference yield: 75.0%

2-<1'-(Diphenylacetoxy)-2',2'-diphenylethenyl>-1-methyl-benzimidazole (57301-63-0) → diphenylacetylhydrazine (6636-02-8) + 2-(Diphenylacetyl)-1-methylbenzimidazole (57301-77-6)

Guidance literature:

With hydrazine hydrate; In methanol; Heating;

DOI:10.1021/jo01300a056

Reference yield:

ethyl diphenylacetate (3468-99-3) → diphenylacetylhydrazine (6636-02-8)

Guidance literature:

With hydrazine hydrate;

upstream raw materials:

diphenylacetic acid chloride

ethyl diphenylacetate

2-<1'-(Diphenylacetoxy)-2',2'-diphenylethenyl>-1-methyl-benzimidazole

hydrazine hydrate

Downstream raw materials:

N,N'-bis-diphenylacetyl-hydrazine

N'-acetyl-2,2-diphenylacetohydrazide

N'-(2,2'-dipehnylacetyl)benzohydrazide

oxalic acid bis-(N'-diphenylacetyl-hydrazide)

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