2-Propenoic acid, 2-methyl-, 2-[(1-oxo-2-propenyl)oxy]ethyl ester

Base Information

• Chemical Name: 2-Propenoic acid, 2-methyl-, 2-[(1-oxo-2-propenyl)oxy]ethyl ester
• CAS No.: 69040-48-8
• Molecular Formula: C9H12O4
• Molecular Weight: 184.192

Synonyms:2-methacryloyloxyethyl acrylate;2-(acryloyloxy)ethyl methacrylate;acryloyloxyethyl methacrylate;MAEA;ethylene glycol acrylate methacrylate;2-Propenoic acid, 2-methyl-, 2-[(1-oxo-2-propenyl)oxy]ethyl ester;EGAMA;

Chemical Property of 2-Propenoic acid, 2-methyl-, 2-[(1-oxo-2-propenyl)oxy]ethyl ester

Chemical Property:

• PSA: 52.60000
• LogP: 0.83490

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 2-methyl-, 2-[(1-oxo-2-propenyl)oxy]ethyl ester

There total 3 articles about 2-Propenoic acid, 2-methyl-, 2-[(1-oxo-2-propenyl)oxy]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

2-methyl-2-propenoic acid 2-hydroxyethyl ester (868-77-9,141668-69-1,25736-86-1,82601-55-6,25249-16-5) + acryloyl chloride (814-68-6,25189-84-8) → ethylene glycol acrylate methacrylate (69040-48-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ja9037406

Reference yield:

Methacryloyl chloride (920-46-7,26937-45-1) + 2-hydroxyethyl acrylate (818-61-1,9051-31-4,26022-14-0) → ethylene glycol acrylate methacrylate (69040-48-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 30.5h;

Reference yield:

→ ethylene glycol acrylate methacrylate (69040-48-8)

Guidance literature:

β-Hydroxyethyl-methacrylat, Acroylchlorid in Dimethylacetamid, α-Nitroso-β-naphthol, 90 Min., 70grad;

upstream raw materials:

2-methyl-2-propenoic acid 2-hydroxyethyl ester

acryloyl chloride

Methacryloyl chloride

2-hydroxyethyl acrylate

Downstream raw materials:

C₂₂H₃₄NO₇P

[Pd(C(Et)HC(O)OCH2CH2OC(O)C(Me)CH2)(dmso)(κ2-(P,O)-2-(2-MeOC6H4)2PC6H4SO3)]

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