Pyrrolo[1,2-c]pyrimidine-2,4(1H)-dicarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]imino]-3,5,6,7-tetrahydro-3-[9-[(4-meth oxyphenyl)methoxy]nonyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, (3R)-

Base Information

Chemical Name:Pyrrolo[1,2-c]pyrimidine-2,4(1H)-dicarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]imino]-3,5,6,7-tetrahydro-3-[9-[(4-meth oxyphenyl)methoxy]nonyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, (3R)-
CAS No.:691006-69-6
Molecular Formula:C36H55N3O8
Molecular Weight:657.848
Hs Code.:

Pyrrolo[1,2-c]pyrimidine-2,4(1H)-dicarboxylic acid,
1-[[(1,1-dimethylethoxy)carbonyl]imino]-3,5,6,7-tetrahydro-3-[9-[(4-meth
oxyphenyl)methoxy]nonyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, (3R)-

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Chemical Property of Pyrrolo[1,2-c]pyrimidine-2,4(1H)-dicarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]imino]-3,5,6,7-tetrahydro-3-[9-[(4-meth oxyphenyl)methoxy]nonyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, (3R)-

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Technology Process of Pyrrolo[1,2-c]pyrimidine-2,4(1H)-dicarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]imino]-3,5,6,7-tetrahydro-3-[9-[(4-meth oxyphenyl)methoxy]nonyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, (3R)-

There total 1 articles about Pyrrolo[1,2-c]pyrimidine-2,4(1H)-dicarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]imino]-3,5,6,7-tetrahydro-3-[9-[(4-meth oxyphenyl)methoxy]nonyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, (3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18107-18-1
diazomethyl-trimethyl-silane

: 874349-39-0
1-tert-butoxycarbonylimino-3-[9-(4-methoxy-benzyloxy)-nonyl]-3,5,6,7-tetrahydro-pyrrolo[1,2-c]pyrimidine-2,4-dicarboxylic acid 2-tert-butyl ester

: 691006-69-6
1-tert-butoxycarbonylimino-3-[9-(4-methoxy-benzyloxy)-nonyl]-3,5,6,7-tetrahydro-pyrrolo[1,2-c]pyrimidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

Guidance literature:: In water; tert-butyl alcohol;
DOI:10.1002/anie.200353200

Reference yield:

: 691006-69-6
1-tert-butoxycarbonylimino-3-[9-(4-methoxy-benzyloxy)-nonyl]-3,5,6,7-tetrahydro-pyrrolo[1,2-c]pyrimidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

: 874349-39-0
1-tert-butoxycarbonylimino-3-[9-(4-methoxy-benzyloxy)-nonyl]-3,5,6,7-tetrahydro-pyrrolo[1,2-c]pyrimidine-2,4-dicarboxylic acid 2-tert-butyl ester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium n-propylmercaptide;
DOI:10.1002/anie.200353200

Reference yield:

: 691006-69-6
1-tert-butoxycarbonylimino-3-[9-(4-methoxy-benzyloxy)-nonyl]-3,5,6,7-tetrahydro-pyrrolo[1,2-c]pyrimidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

: 691006-87-8
C₅₀H₈₀N₆O₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: nPrSLi / hexamethylphosphoric acid triamide / 1.33 h / 20 °C

2: 45.3 mg / Et₃N; BOPCl / CH₂Cl₂ / 12 h / 20 °C

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; lithium n-propylmercaptide; triethylamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1002/chem.200500852