2-(4-Methylphenyl)-2H-1,3-benzodithiole

Base Information

Chemical Name:2-(4-Methylphenyl)-2H-1,3-benzodithiole
CAS No.:69159-75-7
Molecular Formula:C14H12S2
Molecular Weight:244.381
Hs Code.:
DSSTox Substance ID:DTXSID90499101
Nikkaji Number:J793.124G
Wikidata:Q82349600

Synonyms:2-(4-Methylphenyl)-2H-1,3-benzodithiole;69159-75-7;DTXSID90499101

Suppliers and Price of 2-(4-Methylphenyl)-2H-1,3-benzodithiole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(4-Methylphenyl)-2H-1,3-benzodithiole

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:244.03804273
Heavy Atom Count:16
Complexity:219

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2SC3=CC=CC=C3S2

Technology Process of 2-(4-Methylphenyl)-2H-1,3-benzodithiole

There total 6 articles about 2-(4-Methylphenyl)-2H-1,3-benzodithiole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 186707-19-7
3-(4-methylphenyl)-1,2,4-benzotrithiin

: 69159-75-7
2-(4-methylphenyl)-1,3-benzodithiole

Guidance literature:: With triphenylphosphine; In dichloromethane; at 25 ℃; for 4h;
DOI:10.3987/com-95-s7

Reference yield:

: 186707-16-4
3-(4-methylphenyl)-1,2,4,5-benzotetrathiepin

: 69159-75-7
2-(4-methylphenyl)-1,3-benzodithiole

: 186707-19-7
3-(4-methylphenyl)-1,2,4-benzotrithiin

Guidance literature:: With triphenylphosphine; In dichloromethane; at 25 ℃; for 4h;
DOI:10.3987/com-95-s7

Reference yield:

: 17071-97-5
5,6,7,8,9-pentathiabenzocycloheptene

: 69159-75-7
2-(4-methylphenyl)-1,3-benzodithiole

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent Spectr_. / sodium hydride / CH₂Cl₂ / 4 h / 25 °C

2: 94 percent / triphenylphosphine / CH₂Cl₂ / 4 h / 25 °C

With sodium hydride; triphenylphosphine; In dichloromethane;
DOI:10.3987/com-95-s7