Dec-4-YN-1-OL

Base Information

• Chemical Name: Dec-4-YN-1-OL
• CAS No.: 69222-06-6
• Molecular Formula: C10H18O
• Molecular Weight: 154.252
• DSSTox Substance ID: DTXSID70505714
• Wikidata: Q82361002
• Mol file: 69222-06-6.mol

Synonyms:4-Decyn-1-ol;DEC-4-YN-1-OL;69222-06-6;4-decine-1-ol;SCHEMBL879891;DTXSID70505714

Chemical Property of Dec-4-YN-1-OL

Chemical Property:

• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 154.135765193
• Heavy Atom Count: 11
• Complexity: 126

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCC#CCCCO

Technology Process of Dec-4-YN-1-OL

There total 2 articles about Dec-4-YN-1-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-decyn-1-ol (4117-14-0) → 3-decyn-1-ol (51721-39-2) + 4-decyne-1-ol (69222-06-6) + dec-5-yn-1-ol (68274-97-5) + dec-6-yn-1-ol (69222-07-7) + 7-decyn-1-ol (69222-08-8) + 8-decyn-1-ol

Guidance literature:

With sodium 1,3-diaminopropane; In various solvent(s); at 0 ℃; for 0.25h; Product distribution; other times and temperature;

Reference yield:

dec-5-yn-1-ol (68274-97-5) → 3-decyn-1-ol (51721-39-2) + 2-decyn-1-ol (4117-14-0) + 4-decyne-1-ol (69222-06-6) + dec-6-yn-1-ol (69222-07-7) + 7-decyn-1-ol (69222-08-8) + 9-decyn-1-ol (17643-36-6)

Guidance literature:

With sodium 1,3-diaminopropane; In various solvent(s); at 50 ℃; for 4h; Product distribution; other times and temperature;

Reference yield: 99.0%

4-decyne-1-ol (69222-06-6) → (Z)-4-decen-1-ol (57074-37-0)

Guidance literature:

With quinoline; 5% Pd-CaCO3; hydrogen; In hexane; at 20 ℃; for 1h; under 760.051 Torr; stereoselective reaction;

DOI:10.1055/s-0034-1379977

upstream raw materials:

2-decyn-1-ol

dec-5-yn-1-ol

Downstream raw materials:

9-decyn-1-ol

(Z)-4-decen-1-ol

(Z)-6-heneicosen-11-one

11-tosyl-11-heneicos-6Z-enyl isocyanide