7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Base Information

Chemical Name:7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
CAS No.:69703-26-0
Molecular Formula:C28H42N2O6
Molecular Weight:502.651
Hs Code.:
Mol file:69703-26-0.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Technology Process of 7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

There total 1 articles about 7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 824-94-2
p-methoxybenzyl chloride

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 69703-26-0
7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctatetradecane

Guidance literature:: With sodium carbonate; In acetonitrile; Heating;
DOI:10.1021/jo00232a021

Reference yield: 99.0%

: 69703-26-0
7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctatetradecane

: niobium(V) oxide

: 7664-39-3,12381-92-9,32057-09-3,74835-82-8
hydrogen fluoride

: 7732-18-5
water

: (7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane(+2H))(NbF₆)2*2H₂O

Guidance literature:: In methanol; hydrogen fluoride; aq. HF; Nb2O5 was added to 45% HF, soln. was boiled till the volume of 4-5 ml was reached, to the soln. was added soln. of ligand in MeOH; evapn. in vac., resulting crystals were removed before soln. was completely evapd.; elem. anal.;
DOI:10.1039/b902953b

Reference yield: 99.0%

: 69703-26-0
7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctatetradecane

: tantalum(V) oxide

: 7664-39-3,12381-92-9,32057-09-3,74835-82-8
hydrogen fluoride

: 7732-18-5
water

: (7,16-bis(4-methoxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane(+2H))(TaF₆)2*2H₂O

Guidance literature:: In methanol; hydrogen fluoride; aq. HF; Ta2O5 was added to 45% HF, soln. was boiled till the volume of 4-5 ml was reached, to the soln. was added soln. of ligand in MeOH; evapn. in vac., crystals removed before solvent was completely evapd.; elem. anal.;
DOI:10.1039/b902953b