7-HYDROXY-2,2-DIPHENYL-BENZO[1,3]DIOXOLE-5-CARBOXYLIC ACID METHYL ESTER

Base Information

Chemical Name:7-HYDROXY-2,2-DIPHENYL-BENZO[1,3]DIOXOLE-5-CARBOXYLIC ACID METHYL ESTER
CAS No.:69829-46-5
Molecular Formula:C21H16O5
Molecular Weight:348.355
Hs Code.:
Mol file:69829-46-5.mol

Synonyms:methyl 7-hydroxy-2,2-diphenylbenzo[d][1,3]dioxole-5-carboxylate;methyl 3-hydroxy-4,5-(diphenylmethylenedioxy)benzoate;7-hydroxy-2,2-diphenyl-benzo[1,3]dioxole-5-carboxylic acid methyl ester;7-Hydroxy-2,2-diphenyl-benzo[1,3]dioxol-5-carbonsaeure-methylester;methyl 3-hydroxy-4,5-diphenylmethylenedioxybenzoate;

Suppliers and Price of 7-HYDROXY-2,2-DIPHENYL-BENZO[1,3]DIOXOLE-5-CARBOXYLIC ACID METHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
7-HYDROXY-2,2-DIPHENYL-BENZO(1,3)DIOXOLE-5-CARBOXYLIC ACID METHYL ESTER Aldrich
1ea
$ 57.00

Total 5 raw suppliers

Chemical Property of 7-HYDROXY-2,2-DIPHENYL-BENZO[1,3]DIOXOLE-5-CARBOXYLIC ACID METHYL ESTER

Chemical Property:

PSA：64.99000
LogP:3.85130

Purity/Quality:

99% ^*data from raw suppliers

7-HYDROXY-2,2-DIPHENYL-BENZO(1,3)DIOXOLE-5-CARBOXYLIC ACID METHYL ESTER Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 7-HYDROXY-2,2-DIPHENYL-BENZO[1,3]DIOXOLE-5-CARBOXYLIC ACID METHYL ESTER

There total 4 articles about 7-HYDROXY-2,2-DIPHENYL-BENZO[1,3]DIOXOLE-5-CARBOXYLIC ACID METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2051-90-3
Dichlorodiphenylmethane

: 99-24-1
methyl galloate

: 69829-46-5
methyl 7-hydroxy-2,2-diphenylbenzo[d]-1,3-dioxole-5-carboxylate

Guidance literature:: at 170 ℃;
DOI:10.1016/j.tet.2009.08.015

Reference yield:

: 2051-90-3
Dichlorodiphenylmethane

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 69829-46-5
methyl 7-hydroxy-2,2-diphenylbenzo[d]-1,3-dioxole-5-carboxylate

Guidance literature:: With potassium carbonate;

Reference yield:

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 69829-46-5
methyl 7-hydroxy-2,2-diphenylbenzo[d]-1,3-dioxole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / sulfuric acid / 6 h / Heating

2: 62 percent / potassium carbonate / acetonitrile / 16 h / 20 °C

With sulfuric acid; potassium carbonate; In acetonitrile;
DOI:10.1016/j.tet.2004.11.083