Ethyl 4-(benzyloxy)but-2-enoate

Base Information

Chemical Name:Ethyl 4-(benzyloxy)but-2-enoate
CAS No.:70150-60-6
Molecular Formula:C13H16O3
Molecular Weight:220.268
Hs Code.:
DSSTox Substance ID:DTXSID40705784

Synonyms:Ethyl 4-(benzyloxy)but-2-enoate;70150-60-6;DTXSID40705784;AVFZSZKFMFOGQL-UHFFFAOYSA-N;4-Benzyloxy-but-2-enoic acid ethyl ester

Suppliers and Price of Ethyl 4-(benzyloxy)but-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethyl 4-(benzyloxy)but-2-enoate

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:220.109944368
Heavy Atom Count:16
Complexity:217

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C=CCOCC1=CC=CC=C1

Technology Process of Ethyl 4-(benzyloxy)but-2-enoate

There total 18 articles about Ethyl 4-(benzyloxy)but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 60656-87-3
benzyloxyacetoaldehyde

: 70150-60-6
ethyl 2E-4-(benzyloxy)-2-butenoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile;
DOI:10.1016/S0040-4039(96)02121-1

Reference yield: 85.2%

: 4341-76-8
Ethyl 2-butynoate

: 100-51-6,185532-71-2
benzyl alcohol

: 70150-60-6
ethyl 2E-4-(benzyloxy)-2-butenoate

Guidance literature:: With acetic acid; triphenylphosphine; In toluene; at 80 ℃;

Reference yield: 72.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 60656-87-3
benzyloxyacetoaldehyde

: 70150-60-6
ethyl 2E-4-(benzyloxy)-2-butenoate

: 190005-08-4
(Z)-ethyl 4-(benzyloxy)but-2-enoate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at -10 ℃; for 0.5h; Inert atmosphere;

benzyloxyacetoaldehyde; In tetrahydrofuran; mineral oil; at -10 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1002/anie.201705575