N-o-Tolyl-nicotinamide

Base Information

Chemical Name:N-o-Tolyl-nicotinamide
CAS No.:70301-25-6
Molecular Formula:C13H12N2O
Molecular Weight:212.251
Hs Code.:

Synonyms:

Suppliers and Price of N-o-Tolyl-nicotinamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-o-Tolyl-nicotinamide

Chemical Property:

PSA：41.99000
LogP:2.71530

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-o-Tolyl-nicotinamide

There total 6 articles about N-o-Tolyl-nicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 88-72-2
1-methyl-2-nitrobenzene

: 98-92-0,1255150-40-3
nicotinamide

: 70301-25-6
N-(o-tolyl)nicotinamide

Guidance literature:: With carbon monoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; selenium; In toluene; at 160 ℃; for 4h; under 22502.3 Torr;
DOI:10.1002/adsc.200404077

Reference yield: 82.0%

: 626-55-1,163928-56-1
3-Bromopyridine

: 95-53-4
o-toluidine

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 70301-25-6
N-(o-tolyl)nicotinamide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 120 ℃; for 3h; Sealed tube; Inert atmosphere;
DOI:10.1055/s-0037-1609152

Reference yield: 65.0%

: 95-49-8
2-methylchlorobenzene

: 98-92-0,1255150-40-3
nicotinamide

: 70301-25-6
N-(o-tolyl)nicotinamide

Guidance literature:: With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; potassium carbonate; In 1,4-dioxane; at 90 ℃; for 18h; Inert atmosphere; Glovebox;
DOI:10.1002/chem.201302453