1-Phenyl-2-(9-phenyl-9H-purin-6-yl)ethan-1-one

Base Information

Chemical Name:1-Phenyl-2-(9-phenyl-9H-purin-6-yl)ethan-1-one
CAS No.:70386-35-5
Molecular Formula:C₁₉H₁₄N₄O
Molecular Weight:314.346
Hs Code.:
DSSTox Substance ID:DTXSID60499552
Nikkaji Number:J462.427K
Wikidata:Q82350412

Synonyms:1-phenyl-2-(9-phenyl-9H-purin-6-yl)ethanone;70386-35-5;1-Phenyl-2-(9-phenyl-9H-purin-6-yl)ethan-1-one;DTXSID60499552

Suppliers and Price of 1-Phenyl-2-(9-phenyl-9H-purin-6-yl)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Phenyl-2-(9-phenyl-9H-purin-6-yl)ethan-1-one

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:314.11676108
Heavy Atom Count:24
Complexity:431

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)CC2=C3C(=NC=N2)N(C=N3)C4=CC=CC=C4

Technology Process of 1-Phenyl-2-(9-phenyl-9H-purin-6-yl)ethan-1-one

There total 12 articles about 1-Phenyl-2-(9-phenyl-9H-purin-6-yl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 140421-33-6
6-methyl-9-phenyl-9H-purine

: 70386-35-5
phenyl (9-phenyl-9H-purin-6-yl)methyl ketone

Guidance literature:: With sodium hydride; In tetrahydrofuran; Heating;
DOI:10.1248/cpb.40.227

Reference yield:

: 5470-24-6
6-Chloro-9-phenyl-9H-purine

: 70386-35-5
phenyl (9-phenyl-9H-purin-6-yl)methyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / triethylamine / bis(triphenylphosphino)palladium chloride, CuI / dimethylformamide / 5 h / Heating

2: toluene / 60 h / Heating

3: oxalic acid, water / diethyl ether; ethanol / 6 h / Heating

With water; oxalic acid; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In diethyl ether; ethanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 119980-74-4
6-iodo-9-phenyl-9H-purine

: 70386-35-5
phenyl (9-phenyl-9H-purin-6-yl)methyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / triethylamine / bis(triphenylphosphino)palladium chloride, CuI / dimethylformamide / 5 h / Ambient temperature

2: toluene / 60 h / Heating

3: oxalic acid, water / diethyl ether; ethanol / 6 h / Heating

With water; oxalic acid; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In diethyl ether; ethanol; N,N-dimethyl-formamide; toluene;