1-Methyl-4-[(2-phenyl-2-propen-1-yl)sulfinyl]benzene

Base Information

Chemical Name:1-Methyl-4-[(2-phenyl-2-propen-1-yl)sulfinyl]benzene
CAS No.:70411-75-5
Molecular Formula:C16H16OS
Molecular Weight:256.368
Hs Code.:
DSSTox Substance ID:DTXSID501216823

Synonyms:1-Methyl-4-[(2-phenyl-2-propen-1-yl)sulfinyl]benzene;SCHEMBL20925336;DTXSID501216823;70411-75-5

Suppliers and Price of 1-Methyl-4-[(2-phenyl-2-propen-1-yl)sulfinyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Methyl-4-[(2-phenyl-2-propen-1-yl)sulfinyl]benzene

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:256.09218630
Heavy Atom Count:18
Complexity:296

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)CC(=C)C2=CC=CC=C2

Technology Process of 1-Methyl-4-[(2-phenyl-2-propen-1-yl)sulfinyl]benzene

There total 5 articles about 1-Methyl-4-[(2-phenyl-2-propen-1-yl)sulfinyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 6873-55-8
p-tolylsulfinyl amide

: 98-83-9,6144-04-3,25014-31-7,42612-14-6
isopropenylbenzene

: 70411-75-5
1-methyl-4-[(2-phenyl-2-propenyl)sulfinyl]benzene

Guidance literature:: With chloro-trimethyl-silane; ytterbium(III) triflate; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1055/s-2004-820054

Reference yield:

: 10439-23-3
4-methylbenzenesulfinyl chloride

: 70411-75-5
1-methyl-4-[(2-phenyl-2-propenyl)sulfinyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 2.4 g / ammonia / diethyl ether / -78 - 20 °C

2: 34 percent / Yb(OTf)3; TMSCl / CH₂Cl₂; tetrahydrofuran / 48 h / 20 °C

With chloro-trimethyl-silane; ammonia; ytterbium(III) triflate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo035518a

Reference yield:

: 536-57-2
p-toluene sulfinic acid

: 70411-75-5
1-methyl-4-[(2-phenyl-2-propenyl)sulfinyl]benzene

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / diethyl ether / 3 h / 20 °C

2: 2.4 g / ammonia / diethyl ether / -78 - 20 °C

3: 34 percent / Yb(OTf)3; TMSCl / CH₂Cl₂; tetrahydrofuran / 48 h / 20 °C

With chloro-trimethyl-silane; thionyl chloride; ammonia; ytterbium(III) triflate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo035518a