2-(3-Methylbut-2-en-1-yl)cyclohexan-1-one

Base Information

Chemical Name:2-(3-Methylbut-2-en-1-yl)cyclohexan-1-one
CAS No.:704-99-4
Molecular Formula:C11H18O
Molecular Weight:166.263
Hs Code.:
DSSTox Substance ID:DTXSID60505783
Nikkaji Number:J2.832.793E

Synonyms:704-99-4;2-(3-Methylbut-2-en-1-yl)cyclohexan-1-one;SCHEMBL11742664;DTXSID60505783;AKOS010640860

Suppliers and Price of 2-(3-Methylbut-2-en-1-yl)cyclohexan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-(3-Methylbut-2-en-1-yl)cyclohexan-1-one

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:166.135765193
Heavy Atom Count:12
Complexity:187

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CCC1CCCCC1=O)C

Technology Process of 2-(3-Methylbut-2-en-1-yl)cyclohexan-1-one

There total 20 articles about 2-(3-Methylbut-2-en-1-yl)cyclohexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 870-63-3
prenyl bromide

: 704-99-4
2-(3-methylbut-2-en-1-yl)cyclohexanone

Guidance literature:: cyclohexanone; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

prenyl bromide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4.5h; Inert atmosphere;
DOI:10.1021/jacs.8b01005

Reference yield: 78.0%

: 670-80-4
4-cyclohexen-1-ylmorpholine

: 115-18-4
2-methyl-3-buten-2-ol

: 704-99-4
2-(3-methylbut-2-en-1-yl)cyclohexanone

Guidance literature:: With palladium diacetate; triphenylphosphine; zinc dibromide; In dichloromethane; for 5h; regioselective reaction; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2017.05.024