2-(4-Methylcyclohexylidene)acetaldehyde

Base Information

• Chemical Name: 2-(4-Methylcyclohexylidene)acetaldehyde
• CAS No.: 7071-18-3
• Molecular Formula: C9H14O
• Molecular Weight: 138.21
• DSSTox Substance ID: DTXSID401278741
• Nikkaji Number: J2.934.548A
• Mol file: 7071-18-3.mol

Synonyms:2-(4-Methylcyclohexylidene)acetaldehyde;7071-18-3;DTXSID401278741;(4-methylcyclohexylidene)acetaldehyde;2-(4-methyl-cyclohexylidene)-acetaldehyde

Chemical Property of 2-(4-Methylcyclohexylidene)acetaldehyde

Chemical Property:

• XLogP3: 2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 138.104465066
• Heavy Atom Count: 10
• Complexity: 137

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1CCC(=CC=O)CC1

Technology Process of 2-(4-Methylcyclohexylidene)acetaldehyde

There total 15 articles about 2-(4-Methylcyclohexylidene)acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methylcyclohexan-4-one (589-92-4) → (aR)-(-)-(4-methylcyclohexylidene)acetaldehyde (7071-18-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / 1,2-dimethoxy-ethane / 0.75 h / 25 - 30 °C

2: 90 percent / aq. KOH_. CH₃OH / 0.5 h / Heating

With potassium hydroxide; sodium hydride; In 1,2-dimethoxyethane;

DOI:10.1021/ja00348a048

Reference yield:

1-methylcyclohexan-4-one (589-92-4) → (4-Methyl-cyclohexylidene)-acetaldehyde (7071-18-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / 1,2-dimethoxy-ethane / 0.75 h / 25 - 30 °C

2: 90 percent / aq. KOH_. CH₃OH / 0.5 h / Heating

With potassium hydroxide; sodium hydride; In 1,2-dimethoxyethane;

DOI:10.1021/ja00348a048

Reference yield:

1-methylcyclohexan-4-one (589-92-4) → 2-(4-methylcyclohexylidene)acetaldehyde (7071-18-3,85048-14-2,102633-54-5)

Guidance literature:

upstream raw materials:

1-methylcyclohexan-4-one

1-Brom-2-<4-methyl-cyclohexyliden>-aethan

2-(4-Methylcyclohexyliden)-ethanol

ethyl 4-methylcyclohexylideneacetate

Downstream raw materials:

Formic acid 4-methyl-cyclohexylidenemethyl ester

Formic acid 6-methyl-1-oxa-spiro[2.5]oct-2-yl ester

4-methylcyclohexanecarbaldehyde

(Z)-4-((aS)-4-methylcyclohexylidene)-2-butenenitrile