1,4-Bis(4-methylphenyl)anthracene-9,10-dione

Base Information

Chemical Name:1,4-Bis(4-methylphenyl)anthracene-9,10-dione
CAS No.:70866-25-0
Molecular Formula:C28H20O2
Molecular Weight:388.466
Hs Code.:
DSSTox Substance ID:DTXSID80600047
Nikkaji Number:J3.439.707D
Wikidata:Q82496008

Synonyms:70866-25-0;1,4-Di-p-tolylanthracene-9,10-dione;1,4-Bis(4-methylphenyl)anthracene-9,10-dione;SCHEMBL9018851;DTXSID80600047

Suppliers and Price of 1,4-Bis(4-methylphenyl)anthracene-9,10-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-Bis(4-methylphenyl)anthracene-9,10-dione

Chemical Property:

XLogP3:6.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:388.146329876
Heavy Atom Count:30
Complexity:581

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2=C3C(=C(C=C2)C4=CC=C(C=C4)C)C(=O)C5=CC=CC=C5C3=O

Technology Process of 1,4-Bis(4-methylphenyl)anthracene-9,10-dione

There total 4 articles about 1,4-Bis(4-methylphenyl)anthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 85392-80-9
1,4-dibromoanthracene-9,10-dione

: 5720-05-8
4-methylphenylboronic acid

: 70866-25-0
1,4-bis(4-methylphenyl)-9,10-anthracenedione

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; triphenylphosphine; In 1,2-dimethoxyethane; water; at 65 ℃; for 18h; Inert atmosphere;
DOI:10.3390/molecules14031013

Reference yield: 75.0%

: 6119-74-0
1,4-dimethoxyanthraquinone

: 380481-66-3
5,5-dimethyl-2-(4-methylphenyl)-1,3,2-dioxaborinane

: 70866-25-0
1,4-bis(4-methylphenyl)-9,10-anthracenedione

Guidance literature:: With carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); In toluene; at 120 ℃; for 10h; chemoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.7b01666

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 70866-25-0
1,4-bis(4-methylphenyl)-9,10-anthracenedione

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / Inert atmosphere

2: carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II) / toluene / 10 h / 120 °C / Inert atmosphere; Schlenk technique

With carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); In diethyl ether; toluene;
DOI:10.1021/acs.orglett.7b01666