Dodecane-1-sulfinyl chloride

Base Information

• Chemical Name: Dodecane-1-sulfinyl chloride
• CAS No.: 70936-25-3
• Molecular Formula: C12H25ClOS
• Molecular Weight: 252.849
• DSSTox Substance ID: DTXSID80500775
• Nikkaji Number: J1.539.335A
• Mol file: 70936-25-3.mol

Synonyms:70936-25-3;DODECANE-1-SULFINYL CHLORIDE;DTXSID80500775

Chemical Property of Dodecane-1-sulfinyl chloride

Chemical Property:

• XLogP3: 6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 11
• Exact Mass: 252.1314643
• Heavy Atom Count: 15
• Complexity: 151

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCS(=O)Cl

Technology Process of Dodecane-1-sulfinyl chloride

There total 2 articles about Dodecane-1-sulfinyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-dodecyl 2-(trimethylsilyl)ethyl sulfoxide (143505-51-5) → 2-(trimethylsilyl)ethyl chloride (17336-78-6) + 1-dodecanesulfinyl chloride (70936-25-3)

Guidance literature:

With sulfuryl dichloride; In dichloromethane; at -78 - 20 ℃; for 3.5h;

DOI:10.1002/1099-0690(200105)2001:9<1643::aid-ejoc1643>3.0.co;2-m

Reference yield:

N-dodecylsulfanylmethyl-phthalimide (65417-89-2) → N-(chloromethyl)phthalimide (17564-64-6) + 1-dodecanesulfinyl chloride (70936-25-3)

Guidance literature:

With sulfuryl dichloride; acetic anhydride; In tetrachloromethane; for 1h; Yield given; Ambient temperature;

Reference yield:

1-dodecanesulfinyl chloride (70936-25-3) + aniline (62-53-3) → n-Dodecylsulfinylanilid (60140-40-1)

Guidance literature:

In Petroleum ether; Yield given;

upstream raw materials:

N-dodecylsulfanylmethyl-phthalimide

1-dodecyl 2-(trimethylsilyl)ethyl sulfoxide

Downstream raw materials:

n-Dodecylsulfinylanilid