DEUTEROPORPHYRIN IX 2,4 (4,2) HYDROXYETHYL VINYL

Base Information

• Chemical Name: DEUTEROPORPHYRIN IX 2,4 (4,2) HYDROXYETHYL VINYL
• CAS No.: 77222-65-2
• Molecular Formula: C34H36N4O5
• Molecular Weight: 580.684
• Mol file: 77222-65-2.mol

Synonyms:Disperse Yellow 163;

Chemical Property of DEUTEROPORPHYRIN IX 2,4 (4,2) HYDROXYETHYL VINYL

Chemical Property:

• Boiling Point: 1161°Cat760mmHg
• Flash Point: 655.9°C
• PSA: 151.13000
• Density: 1.295g/cm³
• LogP: 3.64660

Purity/Quality:

98% ^*data from raw suppliers

DeuteroporphyrinIX2,4(4,2)hydroxyethylvinyl >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DEUTEROPORPHYRIN IX 2,4 (4,2) HYDROXYETHYL VINYL

There total 2 articles about DEUTEROPORPHYRIN IX 2,4 (4,2) HYDROXYETHYL VINYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hematoporphyrin IX dihydrochloride (17696-69-4,17471-45-3) → 8-(1-hydroxyethyl)-3-vinyldeuteroporphyrin (108331-37-9) + 3-(1-hydroxyethyl)-8-vinyldeuteroporphyrin (77222-65-2) + protoporphyrin IX (553-12-8)

Guidance literature:

With sodium hydroxide; sulfuric acid; acetic acid; Yield given. Multistep reaction. Yields of byproduct given; 2) r.t., 1 h;

DOI:10.1039/c39800001198

Reference yield:

hematoporphyrin IX dihydrochloride (17696-69-4,17471-45-3) → 3-(1-hydroxyethyl)-8-vinyldeuteroporphyrin (77222-65-2) + 3-(1-acetoxyethyl)-8-vinyldeuteroporphyrin + O,O'-diacetylhaematoporphyrin (69423-76-3) + protoporphyrin IX (553-12-8)

Guidance literature:

With sulfuric acid; acetic acid; for 0.25h; Further byproducts given; Ambient temperature; Irradiation;

DOI:10.1039/P19810003135

upstream raw materials:

hematoporphyrin IX dihydrochloride

Refernces

• 1、 Bonnett, Raymond,Ridge, Richard J.,Scourides, Panayiotis A.,Berenbaum, Morris C.. "Haematoporphyrin Derivative". . p. 1198 - 1199. Retrieved 2007/10/02.