(4-Methyl-1-phenylsulfanylpentyl)sulfanylbenzene

Base Information

Chemical Name:(4-Methyl-1-phenylsulfanylpentyl)sulfanylbenzene
CAS No.:71221-29-9
Molecular Formula:C₁₈H₂₂S₂
Molecular Weight:302.505
Hs Code.:
DSSTox Substance ID:DTXSID60500511
Wikidata:Q82352162

Synonyms:71221-29-9;DTXSID60500511;1,1'-[(4-Methylpentane-1,1-diyl)disulfanediyl]dibenzene

Suppliers and Price of (4-Methyl-1-phenylsulfanylpentyl)sulfanylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (4-Methyl-1-phenylsulfanylpentyl)sulfanylbenzene

Chemical Property:

XLogP3:6.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:302.11629305
Heavy Atom Count:20
Complexity:220

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)CCC(SC1=CC=CC=C1)SC2=CC=CC=C2

Technology Process of (4-Methyl-1-phenylsulfanylpentyl)sulfanylbenzene

There total 2 articles about (4-Methyl-1-phenylsulfanylpentyl)sulfanylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3561-67-9
bis(phenylthio)methane

: 107-82-4
i-pentyl bromide

: 71221-29-9
4-methyl-1,1-bisphenylthiopentane

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction;
DOI:10.1016/S0040-4039(00)94317-X

Reference yield:

: 6196-80-1
1-iodo-4-methylpentane

: 3561-67-9
bis(phenylthio)methane

: 71221-29-9
4-methyl-1,1-bisphenylthiopentane

Guidance literature:: With n-butyllithium; In tetrahydrofuran;

Reference yield:

: 71221-29-9
4-methyl-1,1-bisphenylthiopentane

: 88065-33-2
7-methyl-4-phenylthio-octan-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyl-lithium, TMEDA 2.) n-butyl-lithium / 1.) hexane, THF, 0 deg C, 15 min 2.) 30 min, hexane, THF

2: 49 percent / toluene-p-sulphonic acid / benzene / 0.02 h

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; toluene-4-sulfonic acid; In benzene;
DOI:10.1039/P19850001237