Di-tert-butyl 2,3-diazabicyclo[2.2.1]heptane-2,3-dicarboxylate

Base Information

Chemical Name:Di-tert-butyl 2,3-diazabicyclo[2.2.1]heptane-2,3-dicarboxylate
CAS No.:13051-18-8
Molecular Formula:C₁₅H₂₆N₂O₄
Molecular Weight:298.382
Hs Code.:
NSC Number:109898
DSSTox Substance ID:DTXSID10296553

Synonyms:13051-18-8;di-tert-butyl 2,3-diazabicyclo[2.2.1]heptane-2,3-dicarboxylate;NSC109898;DTXSID10296553;NSC-109898

Suppliers and Price of Di-tert-butyl 2,3-diazabicyclo[2.2.1]heptane-2,3-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Di-tert-butyl 2,3-diazabicyclo[2.2.1]heptane-2,3-dicarboxylate

Chemical Property:

Vapor Pressure:5.54E-05mmHg at 25°C
Boiling Point:347°Cat760mmHg
Flash Point:163.7°C
Density:1.14g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:298.18925731
Heavy Atom Count:21
Complexity:396

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)N1C2CCC(C2)N1C(=O)OC(C)(C)C

Technology Process of Di-tert-butyl 2,3-diazabicyclo[2.2.1]heptane-2,3-dicarboxylate

There total 5 articles about Di-tert-butyl 2,3-diazabicyclo[2.2.1]heptane-2,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 39203-22-0
di-tert-butyl 2,3-diazabicyclo[2.2.1]hept-5-ene-2,3-dicarboxylate

: 13051-18-8
2,3-diaza-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid di-tert butyl ester

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; Inert atmosphere;
DOI:10.1021/ja309650u

Reference yield:

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 13051-18-8
2,3-diaza-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid di-tert butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / diethyl ether / 48 h / Ambient temperature

2: 1.96 g / H₂ / platinum dioxide / methanol / 2 h / 760 Torr / Ambient temperature

With hydrogen; platinum(IV) oxide; In methanol; diethyl ether;

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 13051-18-8
2,3-diaza-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid di-tert butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / diethyl ether / 48 h / Ambient temperature

2: 1.96 g / H₂ / platinum dioxide / methanol / 2 h / 760 Torr / Ambient temperature

With hydrogen; platinum(IV) oxide; In methanol; diethyl ether;