Methanedisulfonic acid, [(4-chlorophenyl)hydrazono]-, dipotassium salt

Base Information

• Chemical Name: Methanedisulfonic acid, [(4-chlorophenyl)hydrazono]-, dipotassium salt
• CAS No.: 71366-55-7
• Molecular Formula: C₇H₅ClN₂O₆S₂*2K
• Molecular Weight: 390.908
• Mol file: 71366-55-7.mol

Synonyms:

Chemical Property of Methanedisulfonic acid, [(4-chlorophenyl)hydrazono]-, dipotassium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methanedisulfonic acid, [(4-chlorophenyl)hydrazono]-, dipotassium salt

There total 1 articles about Methanedisulfonic acid, [(4-chlorophenyl)hydrazono]-, dipotassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-aniline (106-47-8) + tripotassium sulfohydrazonomethanedisulfonate (55110-92-4,83285-67-0) → (4-chloro-phenylhydrazono)-methanedisulfonic acid; dipotassium salt (71366-55-7)

Guidance literature:

With hydrogenchloride; potassium nitrite; potassium acetate; Multistep reaction; 1.) from 0 to 15 deg C, 15 min, 2.) 0 deg C, pH 5;

DOI:10.1021/jm00354a023

Reference yield:

(4-chloro-phenylhydrazono)-methanedisulfonic acid; dipotassium salt (71366-55-7) → 3-(4-chlorophenyl)-1,2,3,4-oxatriazol-3-ium-5-olate (71339-71-4)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water;

DOI:10.1039/jr9640000906

Reference yield:

(4-chloro-phenylhydrazono)-methanedisulfonic acid; dipotassium salt (71366-55-7) → C7H4ClN3O7S2(2-)*2K(1+)

Guidance literature:

With sodium nitrite; In water; for 0.5h;

DOI:10.1021/jm00354a023

upstream raw materials:

4-chloro-aniline

tripotassium sulfohydrazonomethanedisulfonate

Downstream raw materials:

3-(4-chlorophenyl)-1,2,3,4-oxatriazol-3-ium-5-olate

Refernces