Cyclopentane, 2-diazo-1,1,3,3-tetramethyl-

Base Information

• Chemical Name: Cyclopentane, 2-diazo-1,1,3,3-tetramethyl-
• CAS No.: 71690-98-7
• Molecular Formula: C9H16N2
• Molecular Weight: 152.239
• DSSTox Substance ID: DTXSID50457161
• Nikkaji Number: J1.545.210B
• Wikidata: Q82279902

Synonyms:71690-98-7;Cyclopentane, 2-diazo-1,1,3,3-tetramethyl-;DTXSID50457161;2,2,5,5-tetramethyldiazocyclopentane;1,1,3,3-Tetramethyl-2-diazocyclopentane

Chemical Property of Cyclopentane, 2-diazo-1,1,3,3-tetramethyl-

Chemical Property:

• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 152.131348519
• Heavy Atom Count: 11
• Complexity: 202

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CCC(C1=[N+]=[N-])(C)C)C

Technology Process of Cyclopentane, 2-diazo-1,1,3,3-tetramethyl-

There total 1 articles about Cyclopentane, 2-diazo-1,1,3,3-tetramethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2,2,5,5-tetramethylcyclopentanone (triphenylphosphoranylidene)hydrazone (70302-23-7) → triphenylphosphine (603-35-0) + 2-Diazo-1,1,3,3-tetramethylcyclopentane (71690-98-7)

Guidance literature:

at 175 ℃; under 0.5 Torr;

DOI:10.1016/S0040-4020(01)96723-7

Reference yield: 10.0%

7-azido-2,4-di-tert-butyl-8,9-thiazabicyclo<4.3.0>nona-2,4,6,9-tetraene (127204-57-3) + 2-Diazo-1,1,3,3-tetramethylcyclopentane (71690-98-7) → 2,4-di-tert-butyl-6-cyanoaniline (17582-88-6) + 2,2,5,5-tetramethyl-1-cyclopentane (138235-27-5) + N,N'-bis(2,4-di-tert-butyl-6-cyanophenyl)sulfur diimide (127204-58-4) + N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide (127616-57-3)

Guidance literature:

In hexane; at 30 ℃; for 48h;

DOI:10.1021/ja00031a043

upstream raw materials:

2,2,5,5-tetramethylcyclopentanone (triphenylphosphoranylidene)hydrazone

Downstream raw materials:

2,4-di-tert-butyl-6-cyanoaniline

2,2,5,5-tetramethyl-1-cyclopentane

N,N'-bis(2,4-di-tert-butyl-6-cyanophenyl)sulfur diimide

N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide

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