Acetic acid, 2,2'-[dithiobis[(2-chloro-4,1-phenylene)oxy]]bis-

Base Information

Chemical Name:Acetic acid, 2,2'-[dithiobis[(2-chloro-4,1-phenylene)oxy]]bis-
CAS No.:719293-89-7
Molecular Formula:C16H12Cl2O6S2
Molecular Weight:435.306
Hs Code.:

Synonyms:

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Chemical Property of Acetic acid, 2,2'-[dithiobis[(2-chloro-4,1-phenylene)oxy]]bis-

Chemical Property:

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Technology Process of Acetic acid, 2,2'-[dithiobis[(2-chloro-4,1-phenylene)oxy]]bis-

There total 4 articles about Acetic acid, 2,2'-[dithiobis[(2-chloro-4,1-phenylene)oxy]]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₀ClN₂O₃⁽¹⁺⁾*Cl^(1-)

: 719293-89-7
4,4'-dithiobis-(2-chlorophenoxyacetic acid)

Guidance literature:: With sodium sulfide; sodium hydroxide; sulfur; In water; at 5 ℃; Heating / reflux;

Reference yield:

: ethyl 2-(2-chloro-4-nitrophenoxy)acetate

: 719293-89-7
4,4'-dithiobis-(2-chlorophenoxyacetic acid)

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / 5%-palladium/activated carbon / ethanol / 3 h

2: hydrogenchloride; sodium nitrite / water / 0.08 h / 5 °C

3: sodium sulfide; sodium hydroxide; sulfur / water / 5 °C / Heating / reflux

With hydrogenchloride; sodium sulfide; sodium hydroxide; hydrogen; sulfur; sodium nitrite; 5%-palladium/activated carbon; In ethanol; water;

Reference yield:

: 619-08-9
2-chloro-4-nitrophenol

: 719293-89-7
4,4'-dithiobis-(2-chlorophenoxyacetic acid)

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / butanone / 10 h / Heating / reflux

2: hydrogen / 5%-palladium/activated carbon / ethanol / 3 h

3: hydrogenchloride; sodium nitrite / water / 0.08 h / 5 °C

4: sodium sulfide; sodium hydroxide; sulfur / water / 5 °C / Heating / reflux

With hydrogenchloride; sodium sulfide; sodium hydroxide; hydrogen; potassium carbonate; sulfur; sodium nitrite; 5%-palladium/activated carbon; In ethanol; water; butanone;