N-(2,4,6-Trimethylphenyl)benzenecarboximidoyl chloride

Base Information

Chemical Name:N-(2,4,6-Trimethylphenyl)benzenecarboximidoyl chloride
CAS No.:72340-40-0
Molecular Formula:C16H16ClN
Molecular Weight:257.763
Hs Code.:
DSSTox Substance ID:DTXSID00502291
Nikkaji Number:J450.167E

Synonyms:N-(2,4,6-Trimethylphenyl)benzenecarboximidoyl chloride;72340-40-0;N-mesitylbenzimidoyl chloride;SCHEMBL13556531;DTXSID00502291

Suppliers and Price of N-(2,4,6-Trimethylphenyl)benzenecarboximidoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,4,6-Trimethylphenyl)benzenecarboximidoyl chloride

Chemical Property:

XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:257.0971272
Heavy Atom Count:18
Complexity:282

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)N=C(C2=CC=CC=C2)Cl)C

Technology Process of N-(2,4,6-Trimethylphenyl)benzenecarboximidoyl chloride

There total 4 articles about N-(2,4,6-Trimethylphenyl)benzenecarboximidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 4476-12-4
N-(2,4,6-trimethylphenyl)benzamide

: 72340-40-0
N-(2,4,6-trimethylphenyl)benzimidoyl chloride

Guidance literature:: With thionyl chloride; at 70 ℃; for 2h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1002/anie.201405027

Reference yield: 98.0%

: 4476-12-4
N-(2,4,6-trimethylphenyl)benzamide

: 72340-40-0
(Z)-N-(2,4,6-trimethylphenyl)benzenecarboximidoyl chloride

Guidance literature:: With thionyl chloride; for 2h; Reflux;
DOI:10.1021/jacs.5b11796

Reference yield:

: 88-05-1
2,4,6-trimethylaniline

: 72340-40-0
N-(2,4,6-trimethylphenyl)benzimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique; Glovebox

2: thionyl chloride / 2 h / 70 °C / Inert atmosphere; Schlenk technique; Glovebox

With thionyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1002/anie.201405027