ethyl 1-(2,6-dichlorophenyl)-2-methylsulfanyl-6-oxo-pyrimidine-5-carbo xylate

Base Information

Chemical Name:ethyl 1-(2,6-dichlorophenyl)-2-methylsulfanyl-6-oxo-pyrimidine-5-carbo xylate
CAS No.:82636-21-3
Molecular Formula:C₁₄H₁₂Cl₂N₂O₃S
Molecular Weight:359.233
Hs Code.:
Mol file:82636-21-3.mol

Synonyms:ETHYL 1-(2,6-DICHLOROPHENYL)-2-METHYLSULFANYL-6-OXO-PYRIMIDINE-5-CARBO XYLATE;

Suppliers and Price of ethyl 1-(2,6-dichlorophenyl)-2-methylsulfanyl-6-oxo-pyrimidine-5-carbo xylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 5 raw suppliers

Chemical Property of ethyl 1-(2,6-dichlorophenyl)-2-methylsulfanyl-6-oxo-pyrimidine-5-carbo xylate

Chemical Property:

Vapor Pressure:5.67E-09mmHg at 25°C
Boiling Point:469.1°Cat760mmHg
PKA:-3.93±0.40(Predicted)
Flash Point:237.5°C
PSA：86.49000
Density:1.44g/cm³
LogP:3.43790

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl 1-(2,6-dichlorophenyl)-2-methylsulfanyl-6-oxo-pyrimidine-5-carbo xylate

There total 4 articles about ethyl 1-(2,6-dichlorophenyl)-2-methylsulfanyl-6-oxo-pyrimidine-5-carbo xylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 27806-81-1
2,6-Dichlorphenyl-S-methylisothioharnstoff

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 82636-21-3
1-(2,6-Dichloro-phenyl)-2-methylsulfanyl-6-oxo-1,6-dihydro-pyrimidine-5-carboxylic acid ethyl ester

Guidance literature:: at 140 ℃; for 20h;

Reference yield:

: 41542-10-3
N-(2,6-dichlorophenyl)-N'-benzoyl thiourea

: 82636-21-3
1-(2,6-Dichloro-phenyl)-2-methylsulfanyl-6-oxo-1,6-dihydro-pyrimidine-5-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / 2,5 N NaOH / 100 °C

2: 66 percent / methanol / Heating

3: 69 percent / 20 h / 140 °C

With sodium hydroxide; In methanol;

Reference yield:

: 608-31-1
2,6-Dichloroaniline

: 82636-21-3
1-(2,6-Dichloro-phenyl)-2-methylsulfanyl-6-oxo-1,6-dihydro-pyrimidine-5-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / benzene

2: 84 percent / 2,5 N NaOH / 100 °C

3: 66 percent / methanol / Heating

4: 69 percent / 20 h / 140 °C

With sodium hydroxide; In methanol; benzene;