1H-Benzo[a]carbazole-1,4(11H)-dione, 11-methyl-

Base Information

Chemical Name:1H-Benzo[a]carbazole-1,4(11H)-dione, 11-methyl-
CAS No.:68452-38-0
Molecular Formula:C17H11NO2
Molecular Weight:261.2747
Hs Code.:
NSC Number:92937
DSSTox Substance ID:DTXSID70293907
Wikidata:Q82032911
ChEMBL ID:CHEMBL1718737

Synonyms:1H-Benzo[a]carbazole-1,4(11H)-dione, 11-methyl-;NSC92937;MLS002701942;68452-38-0;CHEMBL1718737;11-methylbenzo[a]carbazole-1,4-dione;SCHEMBL21945223;DTXSID70293907;BDBM50235876;NSC-92937;1H-Benzo[a]carbazole-1, 11-methyl-;NCI60_042064;SMR001565525

Suppliers and Price of 1H-Benzo[a]carbazole-1,4(11H)-dione, 11-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1H-Benzo[a]carbazole-1,4(11H)-dione, 11-methyl-

Chemical Property:

Vapor Pressure:1.68E-07mmHg at 25°C
Boiling Point:427.1°Cat760mmHg
Flash Point:212.1°C
Density:1.32g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:261.078978594
Heavy Atom Count:20
Complexity:483

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=CC=CC=C2C3=C1C4=C(C=C3)C(=O)C=CC4=O

Technology Process of 1H-Benzo[a]carbazole-1,4(11H)-dione, 11-methyl-

There total 4 articles about 1H-Benzo[a]carbazole-1,4(11H)-dione, 11-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 62747-53-9
1-methyl-3-vinyl-1H-indole

: 106-51-4
p-benzoquinone

: 68452-38-0
NSC92937

Guidance literature:: In ethanol; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.jmedchem.9b00774

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 68452-38-0
NSC92937

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / Inert atmosphere; Cooling with ice

2: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

3: ethanol / 20 °C / Inert atmosphere

With n-butyllithium; sodium hydride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; mineral oil; 2: |Wittig Olefination / 3: |Diels-Alder Cycloaddition;
DOI:10.1021/acs.jmedchem.9b00774

Reference yield:

: 19012-03-4
N-methyl-3-formylindole

: 68452-38-0
NSC92937

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

2: ethanol / 20 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; ethanol; 1: |Wittig Olefination / 2: |Diels-Alder Cycloaddition;
DOI:10.1021/acs.jmedchem.9b00774